Germane, triphenyl(tributylstannyl)-

Base Information

Chemical Name:Germane, triphenyl(tributylstannyl)-
CAS No.:1107-73-9
Molecular Formula:C30H42GeSn
Molecular Weight:593.963
Hs Code.:
Mol file:1107-73-9.mol

Synonyms:

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Chemical Property of Germane, triphenyl(tributylstannyl)-

Chemical Property:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of Germane, triphenyl(tributylstannyl)-

There total 1 articles about Germane, triphenyl(tributylstannyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 3005-32-1
triphenylgermanium bromide

: 813-19-4
bis(tri-n-butyltin)

: 26138-28-3
phenylytterbium iodide

: 1107-73-9
triphenyl(tributylstannyl)butane

: 960-16-7
tributylphenylstannane

Guidance literature:: In tetrahydrofuran; Ar atmosphere, RYbI transferring dropwise under Ar pressure at room temperature, 2 to 3 h, Me3SnCl addn.; extracting with ether, extracts drying (Na2SO4);

Reference yield: 80.0%

: 1107-73-9
triphenyl(tributylstannyl)butane

: 765-46-8
spiro[2.4]hepta-4,6-diene

: 99937-45-8
1-(1,3/1,4-cyclopentadiene-1-yl)-2-(triphenylgermyl)ethan

: 1461-25-2
tetra-n-butyltin(IV)

Guidance literature:: With n-butyllithium; In tetrahydrofuran; triphenyl(tributylstannyl)german reacted with BuLi in THF at -50°C to form triphenylgermyl-Li; the spiro-compd. was added at 0°C, warmed (room temp)., stirred for 3 h, and hydrolyzed (H2O); reactions under N2 in dry, N2-satd. solvent;; evapn., chromy. of the residue on SiO2, eluent CCl4/benzine (2:1), sepn. of tetrabutylstannan as the first fraction; product could not be obtained in pure form because of partial decompn.;;

Reference yield: 76.0%

: 1107-73-9
triphenyl(tributylstannyl)butane

: iron(II) chloride

: 765-46-8
spiro[2.4]hepta-4,6-diene

: 1,1'-bis{2-(triphenylgermyl)ethyl}ferrocene

: 1461-25-2
tetra-n-butyltin(IV)

Guidance literature:: With n-butyllithium; In tetrahydrofuran; triphenyl(tributylstannyl)german reacted with BuLi in THF at -50°C to form triphenylgermyl-Li; the spiro-compd. was added at 0°C, warmed (room temp)., stirred for 1 h, and FeCl2-suspn. in THF added; refluxed for 2 h; hydrolyzed(H2O);; filtration through Na2SO4 and rinsing with CCl4; after evapn., chromy. of the residue on SiO2, eluent CCl4, sepn. of tetrabutylstannan as the first fraction; elem. anal.;;