Technology Process of C48H24F10N6O10
There total 5 articles about C48H24F10N6O10 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
acetonitrile;
for 6h;
Reflux;
DOI:10.1021/jo2024448
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: potassium hydrogencarbonate; potassium iodide / N,N-dimethyl-formamide / 30 °C
2.1: potassium carbonate / N,N-dimethyl-formamide / 60 °C
3.1: sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran / 20 °C
4.1: sodium hydride / N,N-dimethyl-formamide / 3 h / 20 °C
4.2: 6 h / Reflux
5.1: palladium 10% on activated carbon; hydrogen / methanol / 6 h / 20 °C
6.1: potassium carbonate / acetonitrile / 6 h / Reflux
With
sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium(0); palladium 10% on activated carbon; hydrogen; sodium hydride; potassium carbonate; potassium hydrogencarbonate; potassium iodide;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo2024448
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 60 °C
2.1: sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran / 20 °C
3.1: sodium hydride / N,N-dimethyl-formamide / 3 h / 20 °C
3.2: 6 h / Reflux
4.1: palladium 10% on activated carbon; hydrogen / methanol / 6 h / 20 °C
5.1: potassium carbonate / acetonitrile / 6 h / Reflux
With
sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium(0); palladium 10% on activated carbon; hydrogen; sodium hydride; potassium carbonate;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo2024448