C₂₂H₃₁NO₃

Base Information

Chemical Name:C₂₂H₃₁NO₃
CAS No.:1361131-77-2
Molecular Formula:C₂₂H₃₁NO₃
Molecular Weight:357.493
Hs Code.:

C<sub>22</sub>H<sub>31</sub>NO<sub>3</sub>

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Suppliers and Price of C₂₂H₃₁NO₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₃₁NO₃

Chemical Property:

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Technology Process of C₂₂H₃₁NO₃

There total 3 articles about C₂₂H₃₁NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1361131-72-7
C₂₄H₃₃NO₄

: 1361131-77-2
C₂₂H₃₁NO₃

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 6h; Inert atmosphere;
DOI:10.1002/adsc.201100497

Reference yield:

: 2743-40-0
L-leucine ethyl ester hydrochloride

: 1361131-77-2
C₂₂H₃₁NO₃

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate; sodium iodide / tetrahydrofuran; dimethyl sulfoxide / 12 h / Inert atmosphere; Reflux

2: lithium aluminium tetrahydride / tetrahydrofuran / 6 h / 0 °C / Inert atmosphere

With lithium aluminium tetrahydride; sodium hydrogencarbonate; sodium iodide; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1002/adsc.201100497

Reference yield:

: 61-90-5,21675-61-6,25248-98-0,70-45-1
L-leucine

: 1361131-77-2
C₂₂H₃₁NO₃

Guidance literature:: Multi-step reaction with 3 steps

1: chloro-trimethyl-silane / Inert atmosphere

2: sodium hydrogencarbonate; sodium iodide / tetrahydrofuran; dimethyl sulfoxide / 12 h / Inert atmosphere; Reflux

3: lithium aluminium tetrahydride / tetrahydrofuran / 6 h / 0 °C / Inert atmosphere

With lithium aluminium tetrahydride; chloro-trimethyl-silane; sodium hydrogencarbonate; sodium iodide; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1002/adsc.201100497