N,N-bis(phenylmethyl)trimethylgermanecarboselenoamide

Base Information

Chemical Name:N,N-bis(phenylmethyl)trimethylgermanecarboselenoamide
CAS No.:1228095-89-3
Molecular Formula:C₁₈H₂₃GeNSe
Molecular Weight:404.937
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-bis(phenylmethyl)trimethylgermanecarboselenoamide

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Technology Process of N,N-bis(phenylmethyl)trimethylgermanecarboselenoamide

There total 1 articles about N,N-bis(phenylmethyl)trimethylgermanecarboselenoamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1172110-95-0
N,N-dibenzylselenoformamide

: 1529-47-1
chlorotrimethylgermane

: 1228095-89-3
N,N-bis(phenylmethyl)trimethylgermanecarboselenoamide

Guidance literature:: With diisopropylamine; n-BuLi; In tetrahydrofuran; hexane; under Ar; n-BuLi in hexane added at -78°C to soln. of i-Pr2NH in THF; stirred for 30 min; soln. of Se compd. in THF added at -78°C; stirred for 10 min; Me3GeCl added at -78°C; stirred for 24 h; poured into H2O; extd. with Et2O; org. layer dried (MgSO4); filtered; concd. in vac.; subjected to column chromy. (silica gel, hexane-EtOAc 20:1); elem. anal.;
DOI:10.1021/om100290h