C₂₄H₂₂FN₃O₅

Base Information

Chemical Name:C₂₄H₂₂FN₃O₅
CAS No.:906656-89-1
Molecular Formula:C₂₄H₂₂FN₃O₅
Molecular Weight:451.454
Hs Code.:

C<sub>24</sub>H<sub>22</sub>FN<sub>3</sub>O<sub>5</sub>

Synonyms:

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Chemical Property of C₂₄H₂₂FN₃O₅

Chemical Property:

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Technology Process of C₂₄H₂₂FN₃O₅

There total 16 articles about C₂₄H₂₂FN₃O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 906656-55-1
C₂₄H₂₀FN₃O₅

: 906656-89-1
C₂₄H₂₂FN₃O₅

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; N,N-dimethyl-formamide; at 20 ℃; for 20h; Inert atmosphere;
DOI:10.1021/jm301550c

Reference yield:

: 1421314-67-1,906657-94-1
5-benzyloxy-N-(4-fluorobenzyl)-6-formyl-4-oxo-1,4-dihydropyridine-3-carboxamide

: 906656-89-1
C₂₄H₂₂FN₃O₅

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium chlorite; aminosulfonic acid / tetrahydrofuran; water / 1 h / 20 °C / Inert atmosphere; Cooling with ice

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 1.5 h / 20 °C / Inert atmosphere

2.2: 1.5 h / Inert atmosphere; Reflux

3.1: caesium carbonate / N,N-dimethyl-formamide / 4.5 h / 20 °C / Inert atmosphere

4.1: potassium osmate(VI) dihydrate; sodium periodate / 1,4-dioxane / 2 h / 20 °C / Inert atmosphere

5.1: acetic acid / dichloromethane / 0.58 h / 20 - 140 °C / Inert atmosphere; Microwave irradiation

6.1: trifluoroacetic acid / 1.58 h / 20 °C / Inert atmosphere; Cooling with ice

7.1: hydrogen; palladium 10% on activated carbon / methanol; N,N-dimethyl-formamide / 20 h / 20 °C / Inert atmosphere

With potassium osmate(VI) dihydrate; sodium chlorite; sodium periodate; palladium 10% on activated carbon; aminosulfonic acid; hydrogen; benzotriazol-1-ol; caesium carbonate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm301550c

Reference yield:

: 906657-95-2,906658-58-0
3-benzyloxy-5-(4-fluorobenzylcarbamoyl)-4-oxo-1,4-dihydropyridine-2-carboxylic acid

: 906656-89-1
C₂₄H₂₂FN₃O₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 1.5 h / 20 °C / Inert atmosphere

1.2: 1.5 h / Inert atmosphere; Reflux

2.1: caesium carbonate / N,N-dimethyl-formamide / 4.5 h / 20 °C / Inert atmosphere

3.1: potassium osmate(VI) dihydrate; sodium periodate / 1,4-dioxane / 2 h / 20 °C / Inert atmosphere

4.1: acetic acid / dichloromethane / 0.58 h / 20 - 140 °C / Inert atmosphere; Microwave irradiation

5.1: trifluoroacetic acid / 1.58 h / 20 °C / Inert atmosphere; Cooling with ice

6.1: hydrogen; palladium 10% on activated carbon / methanol; N,N-dimethyl-formamide / 20 h / 20 °C / Inert atmosphere

With potassium osmate(VI) dihydrate; sodium periodate; palladium 10% on activated carbon; hydrogen; benzotriazol-1-ol; caesium carbonate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm301550c