(C₆₀HP(C₆H₅)2)Os₃(CO)11

Base Information

Chemical Name:(C₆₀HP(C₆H₅)2)Os₃(CO)11
CAS No.:1207318-61-3
Molecular Formula:C₈₃H₁₁O₁₁Os₃P
Molecular Weight:1785.57
Hs Code.:

(C<sub>60</sub>HP(C<sub>6</sub>H<sub>5</sub>)2)Os<sub>3</sub>(CO)11

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (C₆₀HP(C₆H₅)2)Os₃(CO)11

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Technology Process of (C₆₀HP(C₆H₅)2)Os₃(CO)11

There total 1 articles about (C₆₀HP(C₆H₅)2)Os₃(CO)11 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 133869-39-3,65702-94-5
undecacarbonyl(acetonitrile)triosmium

: 159831-83-1
C₆₀HP(C₆H₅)2

: 1207318-61-3
(C₆₀HP(C₆H₅)2)Os₃(CO)11

Guidance literature:: In dichloromethane; under N2; CH2Cl2 added to (PPh2)C60H and Os complex; stirred at room temp. for 2 h; volatiles removed on rotary evaporator; subjected to TLC (silica gel, CS2); second brown band collected; crystd. from CS2-MeOH; elem. anal.;
DOI:10.1021/om900914a

Reference yield: 72.0%

: 1207318-61-3
(C₆₀HP(C₆H₅)2)Os₃(CO)11

: 1207318-60-2
Os3(CO)10(μ,η3-(PPh2)C60H)

Guidance literature:: In toluene; under N2; Os complex in toluene heated to reflux for 2 h; cooled to roomtemp.; solvent removed under vac.; subjected to TLC (silica gel, CS2);
DOI:10.1021/om900914a