ethyl 3-(2-furyl)-3-hydroxypropanoate

Base Information

Chemical Name:ethyl 3-(2-furyl)-3-hydroxypropanoate
CAS No.:119619-41-9
Molecular Formula:C₉H₁₂O₄
Molecular Weight:184.192
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 3-(2-furyl)-3-hydroxypropanoate

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Technology Process of ethyl 3-(2-furyl)-3-hydroxypropanoate

There total 9 articles about ethyl 3-(2-furyl)-3-hydroxypropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 98-01-1
furfural

: 623-48-3
ethyl iodoacetae

: 119619-41-9,119678-70-5,129101-56-0,25408-95-1
ethyl 3-(2-furyl)-3-hydroxypropanoate

Guidance literature:: ethyl iodoacetae; With air; dimethyl zinc(II); In diethyl ether; toluene; at 0 ℃; for 0.5h;

furfural; With air; Triphenylphosphine oxide; In diethyl ether; toluene; at 0 ℃;
DOI:10.1002/adsc.200700572

Reference yield: 98.0%

: 98-01-1
furfural

: 56579-97-6
lithium 1-ethoxyethenolate

: 119619-41-9,119678-70-5,129101-56-0,25408-95-1
ethyl 3-(2-furyl)-3-hydroxypropanoate

Guidance literature:: In tetrahydrofuran; at -78 - 20 ℃; for 4h; Inert atmosphere;
DOI:10.1016/j.tetlet.2018.05.056

Reference yield: 94.0%

: 98-01-1
furfural

: 141-78-6
ethyl acetate

: 119619-41-9,119678-70-5,129101-56-0,25408-95-1
ethyl 3-(2-furyl)-3-hydroxypropanoate

Guidance literature:: ethyl acetate; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

furfural; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;
DOI:10.1002/ejoc.201100917