3-methyl-1-phenyl-5(4-(acetyl semicarbazone-1-yl)benzene sulfonamido)pyrazole

Base Information

Chemical Name:3-methyl-1-phenyl-5(4-(acetyl semicarbazone-1-yl)benzene sulfonamido)pyrazole
CAS No.:494189-63-8
Molecular Formula:C₁₉H₂₀N₆O₃S
Molecular Weight:412.472
Hs Code.:

Synonyms:

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Chemical Property of 3-methyl-1-phenyl-5(4-(acetyl semicarbazone-1-yl)benzene sulfonamido)pyrazole

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Technology Process of 3-methyl-1-phenyl-5(4-(acetyl semicarbazone-1-yl)benzene sulfonamido)pyrazole

There total 3 articles about 3-methyl-1-phenyl-5(4-(acetyl semicarbazone-1-yl)benzene sulfonamido)pyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 563-41-7
semicarbazide hydrochloride

: 494189-46-7
3-methyl-1-phenyl-5(4-acetyl)sulfonamidophenylpyrazole

: 494189-63-8
3-methyl-1-phenyl-5(4-(acetyl semicarbazone-1-yl)benzene sulfonamido)pyrazole

Guidance literature:: With sodium acetate; In ethanol; water; for 2h; Heating;
DOI:10.1080/10426500210238

Reference yield:

: 1131-18-6
1-Phenyl-3-methyl-5-aminopyrazole

: 494189-63-8
3-methyl-1-phenyl-5(4-(acetyl semicarbazone-1-yl)benzene sulfonamido)pyrazole

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / pyridine / 2 h / Heating

2: 58 percent / NaOAc / ethanol; H₂O / 2 h / Heating

With pyridine; sodium acetate; In ethanol; water;
DOI:10.1080/10426500210238

Reference yield:

: 1788-10-9
4-Acetylbenzenesulfonyl chloride

: 494189-63-8
3-methyl-1-phenyl-5(4-(acetyl semicarbazone-1-yl)benzene sulfonamido)pyrazole

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / pyridine / 2 h / Heating

2: 58 percent / NaOAc / ethanol; H₂O / 2 h / Heating

With pyridine; sodium acetate; In ethanol; water;
DOI:10.1080/10426500210238