Dicyclohexylphosphinyl-N-methyl(thioformamide)

Base Information

Chemical Name:Dicyclohexylphosphinyl-N-methyl(thioformamide)
CAS No.:14633-79-5
Molecular Formula:C₁₄H₂₆NOPS
Molecular Weight:287.406
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Dicyclohexylphosphinyl-N-methyl(thioformamide)

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Technology Process of Dicyclohexylphosphinyl-N-methyl(thioformamide)

There total 1 articles about Dicyclohexylphosphinyl-N-methyl(thioformamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14633-79-5
Dicyclohexylphosphinyl-N-methyl(thioformamide)

Guidance literature:: Dicyclohexyl--phosphin in A. durch Einleiten von Sauerstoff;
DOI:10.1002/zaac.19673510104

Reference yield: 49.0%

: H⁽¹⁺⁾*AuCl₄^(1-)*(2-3)H₂O

: 14633-79-5
Dicyclohexylphosphinyl-N-methyl(thioformamide)

: 163630-47-5
[dicyclohexylphosphinyl-N-methyl(thioformamide)]gold(I) chloride

Guidance literature:: With thiodiglycol; In ethanol; acetone; addn. of thiodiglycol to soln. of Au-compd. (in acetone), then addn. of ligand soln. (in EtOH, pptn.); recrystn. (CH2Cl2); elem. anal.;
DOI:10.1071/CH9950757

Reference yield: 30.0%

: 14633-79-5
Dicyclohexylphosphinyl-N-methyl(thioformamide)

: 639-58-7
triphenyltin chloride

: 172423-55-1
(C₆H₅)3Sn[(C₆H₁₁)2P(O)C(S)N(H)CH₃]Cl

Guidance literature:: In benzene; stirring (3.5 h); solvent evapn., CH2Cl2 addn., centrifugation, evapn., recrystn. (hot EtOH);
DOI:10.1071/CH9951659