palladium(μ-acetato)-3,6-bis(4-pentoxyphenyl)-1,2,4,5-tetrazine

Base Information

Chemical Name:palladium(μ-acetato)-3,6-bis(4-pentoxyphenyl)-1,2,4,5-tetrazine
CAS No.:654671-06-4
Molecular Formula:C₅₂H₆₄N₈O₈Pd₂
Molecular Weight:1141.97
Hs Code.:

Synonyms:

Suppliers and Price of palladium(μ-acetato)-3,6-bis(4-pentoxyphenyl)-1,2,4,5-tetrazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of palladium(μ-acetato)-3,6-bis(4-pentoxyphenyl)-1,2,4,5-tetrazine

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of palladium(μ-acetato)-3,6-bis(4-pentoxyphenyl)-1,2,4,5-tetrazine

There total 2 articles about palladium(μ-acetato)-3,6-bis(4-pentoxyphenyl)-1,2,4,5-tetrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 72243-02-8
3,6-bis(4-pentoxyphenyl)-1,2,4,5-tetrazine

: 3375-31-3
palladium diacetate

: 654671-06-4
palladium(μ-acetato)-3,6-bis(4-pentoxyphenyl)-1,2,4,5-tetrazine

Guidance literature:: In acetic acid; addn. of palladium salt to a soln. of ligand in acetic acid at 60°C, stirring for 16 h; evapn., washing with hexane, dissolving in CHCl3, filtration through Celite, evapn., drying;
DOI:10.1016/j.jorganchem.2003.08.038

Reference yield: 7.0%

: 10025-98-6
potassium tetrachloropalladate(II)

: 72243-02-8
3,6-bis(4-pentoxyphenyl)-1,2,4,5-tetrazine

: di-palladium(chloro)-3,6-bis(4-pentoxyphenyl)-1,2,4,5-tetrazine

: 654671-06-4
palladium(μ-acetato)-3,6-bis(4-pentoxyphenyl)-1,2,4,5-tetrazine

Guidance literature:: In acetic acid; addn. of palladium complex to a soln. of ligand in acetic acid at 60°C, stirring for 16 h; evapn., washing with water, acetone, dissolving in CHCl3, filtration through Celite, evapn., drying in vac.;
DOI:10.1016/j.jorganchem.2003.08.038

Reference yield: 70.0%

: 654671-06-4
palladium(μ-acetato)-3,6-bis(4-pentoxyphenyl)-1,2,4,5-tetrazine

: 1118-67-8
sodium (Z)-4-oxopent-2-en-2-olate

: 654671-05-3
palladium(acetylacetonato)-[3,6-bis(4-pentoxyphenyl)-1,2,4,5-tetrazine]

Guidance literature:: In tetrahydrofuran; addn. of sodium salt to a soln. of palladium complex in THF, stirring atroom temp. for 4 h; evapn., washing with hexane, Et2O, drying;
DOI:10.1016/j.jorganchem.2003.08.038