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Technology Process of Pu(NCS)4(P(CH3)2(C6H5)O)4

Pu(NCS)4(P(CH3)2(C6H5)O)4

Base Information
  • Chemical Name:Pu(NCS)4(P(CH3)2(C6H5)O)4
  • CAS No.:105992-58-3
  • Molecular Formula:C36H44N4O4P4PuS4
  • Molecular Weight:1092.99
  • Hs Code.:
Pu(NCS)4(P(CH<sub>3</sub>)2(C<sub>6</sub>H<sub>5</sub>)O)4

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Technology Process of Pu(NCS)4(P(CH3)2(C6H5)O)4

There total 1 articles about Pu(NCS)4(P(CH3)2(C6H5)O)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

PuCl<sub>4</sub>*2P(CH<sub>3</sub>)2(C<sub>6</sub>H<sub>5</sub>)O

PuCl4*2P(CH3)2(C6H5)O

dimethyl(phenyl)phosphine oxide
10311-08-7

dimethyl(phenyl)phosphine oxide

Pu(NCS)4(P(CH<sub>3</sub>)2(C<sub>6</sub>H<sub>5</sub>)O)4
105992-58-3

Pu(NCS)4(P(CH3)2(C6H5)O)4

Guidance literature:
With potassium thioacyanate; In acetonitrile; stirring Pu complex with potassium thiocyanate (stoichiometric amt.) and phosphine oxide (excess) under N2, 16h; evapn. to dryness; dissoln. in CH2Cl2; addn. of 2-methylbutane; pptn.; washing (2-methylbutane); vacuum drying, 4h; elem. anal.;
DOI:10.1016/0022-5088(86)90666-1

Reference yield: 64.0%

Pu(NCS)4(P(CH<sub>3</sub>)2(C<sub>6</sub>H<sub>5</sub>)O)4
105992-58-3

Pu(NCS)4(P(CH3)2(C6H5)O)4

cyclopentadienylthallium(I)

cyclopentadienylthallium(I)

Pu<sup>(4+)</sup>*C<sub>5</sub>H<sub>5</sub><sup>(1-)</sup>*3NCS<sup>(1-)</sup>*2P(CH<sub>3</sub>)2(C<sub>6</sub>H<sub>5</sub>)O=Pu(C<sub>5</sub>H<sub>5</sub>)(NCS)3*2P(CH<sub>3</sub>)2(C<sub>6</sub>H<sub>5</sub>)O

Pu(4+)*C5H5(1-)*3NCS(1-)*2P(CH3)2(C6H5)O=Pu(C5H5)(NCS)3*2P(CH3)2(C6H5)O

Guidance literature:
In acetonitrile; addn. of stoichiometric amt. of TlC5H5 to Pu complex soln.; stirring overnight; evapn. to dryness under vac.; dissoln. in CH2Cl2; addn. of 2-methylbutane; pptn.; washing (2-methylbutane); vacuum drying, 4h; elem. anal.;
DOI:10.1016/0022-5088(86)90666-1
upstream raw materials:

dimethyl(phenyl)phosphine oxide

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