(C₅H₂(C(CH₃)3)3)2CeCH₂C₆H₄CH₃

Base Information

Chemical Name:(C₅H₂(C(CH₃)3)3)2CeCH₂C₆H₄CH₃
CAS No.:1244030-78-1
Molecular Formula:C₄₂H₆₇Ce
Molecular Weight:712.114
Hs Code.:

(C<sub>5</sub>H<sub>2</sub>(C(CH<sub>3</sub>)3)3)2CeCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>CH<sub>3</sub>

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Chemical Property of (C₅H₂(C(CH₃)3)3)2CeCH₂C₆H₄CH₃

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Technology Process of (C₅H₂(C(CH₃)3)3)2CeCH₂C₆H₄CH₃

There total 2 articles about (C₅H₂(C(CH₃)3)3)2CeCH₂C₆H₄CH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: [bis(1,2,4-tri-t-butylcyclopentadienyl)cerium](CF₃SO₃)*0.5C₆H₁₄

: 29875-07-8
(4-methylbenzyl)magnesium chloride

: 832076-18-3
bis(1,2,4-tri-tert-butylcyclopentadienyl)cerium benzyl

: 1244030-78-1
(C₅H₂(C(CH₃)3)3)2CeCH₂C₆H₄CH₃

Guidance literature:: In diethyl ether; pentane; (Schlenk, inert atm.) Mg-compound in diethyl ether was added to a soln. of complex in pentane, 2 min; the solvent was removed under reduced pressure, extd. with pentane, reduced in vol., cooled to -10°C; elem. anal.;
DOI:10.1039/b918103b

Reference yield:

: 832076-18-3
bis(1,2,4-tri-tert-butylcyclopentadienyl)cerium benzyl

: 106-42-3
para-xylene

: 1244030-78-1
(C₅H₂(C(CH₃)3)3)2CeCH₂C₆H₄CH₃

Guidance literature:: In neat (no solvent); (Schlenk, inert atm.) Ce-compound was dissolved in p-xylene in NMR tube and heated at 60°C for 2 days; taken to dryness, detected by NMR spectra;
DOI:10.1039/b918103b