Technology Process of N-tosyl-(1RS,2SR)-2-<(2SR)-2,3-epoxypropyl>cyclopentylamine
There total 6 articles about N-tosyl-(1RS,2SR)-2-<(2SR)-2,3-epoxypropyl>cyclopentylamine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 46 percent / 25percent aq. NaOH / dimethylformamide; H2O / 1 h / pH 12
2: 1) m-chloroperbenzoic acid, 2) potassium carbonate / 1) chloroform, room temperature, 2) 0 deg C, 2 h
With
sodium hydroxide; potassium carbonate; 3-chloro-benzenecarboperoxoic acid;
In
water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)96036-3
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 46 percent / 25percent aq. NaOH / dimethylformamide; H2O / 1 h / pH 12
2: 1) m-chloroperbenzoic acid, 2) potassium carbonate / 1) chloroform, room temperature, 2) 0 deg C, 2 h
With
sodium hydroxide; potassium carbonate; 3-chloro-benzenecarboperoxoic acid;
In
water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)96036-3
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 6 g / LiAlH4 / diethyl ether
2: 46 percent / 25percent aq. NaOH / dimethylformamide; H2O / 1 h / pH 12
3: 1) m-chloroperbenzoic acid, 2) potassium carbonate / 1) chloroform, room temperature, 2) 0 deg C, 2 h
With
sodium hydroxide; lithium aluminium tetrahydride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid;
In
diethyl ether; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)96036-3