2-dodecylpropane-1,3-diyl bistoluene p-sulfonate

Base Information

Chemical Name:2-dodecylpropane-1,3-diyl bistoluene p-sulfonate
CAS No.:71366-37-5
Molecular Formula:C₂₉H₄₄O₆S₂
Molecular Weight:552.797
Hs Code.:

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Chemical Property of 2-dodecylpropane-1,3-diyl bistoluene p-sulfonate

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Technology Process of 2-dodecylpropane-1,3-diyl bistoluene p-sulfonate

There total 4 articles about 2-dodecylpropane-1,3-diyl bistoluene p-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 10395-09-2
2-dodecylpropane-1,3-diol

: 98-59-9
p-toluenesulfonyl chloride

: 71366-37-5
2-dodecylpropane-1,3-diyl bistoluene p-sulfonate

Guidance literature:: With pyridine;
DOI:10.1021/jo00375a041

Reference yield:

: 7252-87-1
diethyl 2-dodecylmalonate

: 71366-37-5
2-dodecylpropane-1,3-diyl bistoluene p-sulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / LiAlH₄ / diethyl ether

2: 82 percent / pyridine

With pyridine; lithium aluminium tetrahydride; In diethyl ether;
DOI:10.1021/jo00375a041

Reference yield:

: 143-15-7
1-dodecylbromide

: 71366-37-5
2-dodecylpropane-1,3-diyl bistoluene p-sulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 2.)LiAlH₄ / 2.)Et₂O

2: pyridine / 10 °C

With lithium aluminium tetrahydride; In pyridine;
DOI:10.1016/S0040-4039(00)87454-7