4-Nitrobenzyl (1S,5R,6S)-2-[6-(3-t-butyl-dimethylsilyloxy)benzyl-7-methylthioimidazo[5,1-b]-thiazolium-2-yl]-6-((1R)-1-hydroxyethyl)-1-methyl-1-carbapen-2-em3-carboxylate bromide

Base Information

• Chemical Name: 4-Nitrobenzyl (1S,5R,6S)-2-[6-(3-t-butyl-dimethylsilyloxy)benzyl-7-methylthioimidazo[5,1-b]-thiazolium-2-yl]-6-((1R)-1-hydroxyethyl)-1-methyl-1-carbapen-2-em3-carboxylate bromide
• CAS No.: 352308-08-8
• Molecular Formula: Br*C₃₆H₄₃N₄O₇S₂Si
• Molecular Weight: 815.882

Synonyms:

Chemical Property of 4-Nitrobenzyl (1S,5R,6S)-2-[6-(3-t-butyl-dimethylsilyloxy)benzyl-7-methylthioimidazo[5,1-b]-thiazolium-2-yl]-6-((1R)-1-hydroxyethyl)-1-methyl-1-carbapen-2-em3-carboxylate bromide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 4-Nitrobenzyl (1S,5R,6S)-2-[6-(3-t-butyl-dimethylsilyloxy)benzyl-7-methylthioimidazo[5,1-b]-thiazolium-2-yl]-6-((1R)-1-hydroxyethyl)-1-methyl-1-carbapen-2-em3-carboxylate bromide

There total 2 articles about 4-Nitrobenzyl (1S,5R,6S)-2-[6-(3-t-butyl-dimethylsilyloxy)benzyl-7-methylthioimidazo[5,1-b]-thiazolium-2-yl]-6-((1R)-1-hydroxyethyl)-1-methyl-1-carbapen-2-em3-carboxylate bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-t-butyldimethylsilyloxybenzyl bromide + 4-nitrobenzyl (1S,5R,6S)-6-((1R)-1-hydroxyethyl)-1-methyl-2-(7-methylthioimidazo[5,1-b]thiazol-2-yl)-1-carbapen-2-em-3-carboxylate → 4-Nitrobenzyl (1S,5R,6S)-2-[6-(3-t-butyl-dimethylsilyloxy)benzyl-7-methylthioimidazo[5,1-b]-thiazolium-2-yl]-6-((1R)-1-hydroxyethyl)-1-methyl-1-carbapen-2-em3-carboxylate bromide (352308-08-8)

Guidance literature:

Reference yield:

4-nitrobenzyl (1S,5R,6S)-6-((1R)-1-hydroxyethyl)-1-methyl-2-(7-methylthioimidazo-[5,1-b]thiazol-2-yl)-1-carbapen-2-em-3-carboxylate (258840-07-2) + [3-(bromomethyl)-phenoxy]dimethyl(1,1-dimethylethyl)silane (131362-25-9) → 4-Nitrobenzyl (1S,5R,6S)-2-[6-(3-t-butyl-dimethylsilyloxy)benzyl-7-methylthioimidazo[5,1-b]-thiazolium-2-yl]-6-((1R)-1-hydroxyethyl)-1-methyl-1-carbapen-2-em3-carboxylate bromide (352308-08-8)

Guidance literature:

In chloroform; acetonitrile; at 20 ℃;

DOI:10.1016/j.bmcl.2008.11.039

Reference yield:

4-Nitrobenzyl (1S,5R,6S)-2-[6-(3-t-butyl-dimethylsilyloxy)benzyl-7-methylthioimidazo[5,1-b]-thiazolium-2-yl]-6-((1R)-1-hydroxyethyl)-1-methyl-1-carbapen-2-em3-carboxylate bromide (352308-08-8) → Br(1-)*C30H29N4O7S2(1+)

Guidance literature:

With tetrabutyl ammonium fluoride; acetic acid;

DOI:10.1016/j.bmcl.2008.11.039

upstream raw materials:

4-nitrobenzyl (1S,5R,6S)-6-((1R)-1-hydroxyethyl)-1-methyl-2-(7-methylthioimidazo-[5,1-b]thiazol-2-yl)-1-carbapen-2-em-3-carboxylate

[3-(bromomethyl)-phenoxy]dimethyl(1,1-dimethylethyl)silane

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