1-Iodo-1-hexyne

Base Information

• Chemical Name: 1-Iodo-1-hexyne
• CAS No.: 1119-67-1
• Molecular Formula: C6H9I
• Molecular Weight: 208.042
• Hs Code.: 2903399090
• Mol file: 1119-67-1.mol

Synonyms:1-Hexyne, 1-iodo-;1-iodohex-1-yne;

Chemical Property of 1-Iodo-1-hexyne

Chemical Property:

• Flash Point: 67℃
• PSA: 0.00000
• Density: 1.564 at 20 °C
• LogP: 2.57250
• Storage Temp.: 2-8°C

Purity/Quality:

98%,99%, ^*data from raw suppliers

1-IODO-1-HEXYNE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): 1740148
• Hazard Codes: Xi
• Statements: 36/38
• Safety Statements: 26

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of 1-Iodo-1-hexyne

There total 12 articles about 1-Iodo-1-hexyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

hex-1-yne (693-02-7) → 1-iodo-1-hexyne (1119-67-1)

Guidance literature:

With n-butyllithium; iodine; In diethyl ether;

DOI:10.1021/jo100971j

Reference yield: 87.0%

C9H18B(1-)*Li(1+) (121826-88-8) → hept-2-yne (1119-65-9) + 1-iodo-1-hexyne (1119-67-1)

Guidance literature:

With iodine; In tetrahydrofuran; diethyl ether; from -78 deg C to 25 deg C;

DOI:10.1016/S0040-4039(00)80450-5

Reference yield:

1-iodo-2-phenylethyne (932-88-7) + hex-1-yne (693-02-7) → 1-iodo-1-hexyne (1119-67-1) + phenylacetylene (536-74-3)

Guidance literature:

With 2,6-dimethylpyridine; tris-triphenylphosphine copper(I) iodide; at 20 ℃; for 18h;

DOI:10.1021/cs500326e

upstream raw materials:

hexenylmagnesium bromide

hex-1-yne

C₉H₁₈B^(1-)*Li⁽¹⁺⁾

C₁₅H₃₃BO

Downstream raw materials:

1-phenylocta-1,3-diyne

2-[1-Iodo-meth-(Z)-ylidene]-hexanoic acid cyclohexylamide

(5Z)-dodec-5-en-7-yne

(Z)-1-iodohex-1-ene

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