C₃₄H₂₈ClN₄O₃P

Base Information

• Chemical Name: C₃₄H₂₈ClN₄O₃P
• CAS No.: 133031-95-5
• Molecular Formula: C₃₄H₂₈ClN₄O₃P
• Molecular Weight: 607.048
• Mol file: 133031-95-5.mol

Synonyms:

Chemical Property of C₃₄H₂₈ClN₄O₃P

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₄H₂₈ClN₄O₃P

There total 3 articles about C₃₄H₂₈ClN₄O₃P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

C16H13ClN6O3 (133069-27-9) + triphenylphosphine (603-35-0) → C34H28ClN4O3P (133031-95-5)

Guidance literature:

In diethyl ether; for 4h; Heating;

Reference yield:

(2-amino-5-chlorophenyl)(pyridin-4-yl)methanone (105192-42-5) → C34H28ClN4O3P (133031-95-5)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) aq. HCl, acetic acid, sodium nitrite, 2.) sodium acetate / 1.) 0 deg C, 2.) water, ethanol, RT, 3 h

2: 76 percent / sodium azide, hexadecyltributylphosphonium bromide / benzene; H₂O / 24 h / 40 °C

3: 41 percent / diethyl ether / 4 h / Heating

With hydrogenchloride; sodium azide; sodium acetate; cetyltributylphosphonium bromide; acetic acid; sodium nitrite; In diethyl ether; water; benzene;

Reference yield:

C16H13Cl2N3O3 (133031-87-5) → C34H28ClN4O3P (133031-95-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 76 percent / sodium azide, hexadecyltributylphosphonium bromide / benzene; H₂O / 24 h / 40 °C

2: 41 percent / diethyl ether / 4 h / Heating

With sodium azide; cetyltributylphosphonium bromide; In diethyl ether; water; benzene;

upstream raw materials:

C₁₆H₁₃ClN₆O₃

triphenylphosphine

(2-amino-5-chlorophenyl)(pyridin-4-yl)methanone

C₁₆H₁₃Cl₂N₃O₃