2-fluoro-3,6-diiodopyridine

Base Information

• Chemical Name: 2-fluoro-3,6-diiodopyridine
• CAS No.: 1245321-31-6
• Molecular Formula: C₅H₂FI₂N
• Molecular Weight: 348.885

Synonyms:

Chemical Property of 2-fluoro-3,6-diiodopyridine

Chemical Property:

• Boiling Point: 312.0±37.0 °C(Predicted)
• Density: 2.662±0.06 g/cm3(Predicted)

Purity/Quality:

95+% ^*data from raw suppliers

2-Fluoro-3,6-diiodopyridine 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-fluoro-3,6-diiodopyridine

There total 1 articles about 2-fluoro-3,6-diiodopyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

2-fluoropyridine (372-48-5) → 2-fluoro-3,6-diiodopyridine (1245321-31-6) + 2-fluoro-3-iodopyridine (113975-22-7)

Guidance literature:

2-fluoropyridine; With 2,2,6,6-tetramethyl-piperidine; n-butyllithium; zinc dichloro(N,N,N′,N′-tetramethylethylenediamine); In tetrahydrofuran; hexane; at 20 ℃; for 2h; Inert atmosphere;

With iodine; In tetrahydrofuran; hexane; at 20 ℃; Concentration; regioselective reaction; Inert atmosphere;

DOI:10.1016/j.tet.2016.03.022

upstream raw materials:

2-fluoropyridine

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