p-bromoacetophenoneoctahydroroimatacene ester

Base Information

Chemical Name:p-bromoacetophenoneoctahydroroimatacene ester
CAS No.:1315281-46-9
Molecular Formula:C₃₈H₆₅BrO₈
Molecular Weight:729.833
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-bromoacetophenoneoctahydroroimatacene ester

Chemical Property:

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Technology Process of p-bromoacetophenoneoctahydroroimatacene ester

There total 2 articles about p-bromoacetophenoneoctahydroroimatacene ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1315281-45-8
octahydroroimatacene

: 99-73-0,132309-76-3
para-bromophenacyl bromide

: 1315281-46-9
p-bromoacetophenoneoctahydroroimatacene ester

Guidance literature:: With triethylamine; In acetone; at 20 ℃; for 19h; Molecular sieve;
DOI:10.1002/chem.201003677

Reference yield:

: 1316250-71-1
roimatacene

: 1315281-46-9
p-bromoacetophenoneoctahydroroimatacene ester

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 4.5 h / 20 °C

2: triethylamine / acetone / 19 h / 20 °C / Molecular sieve

With palladium 10% on activated carbon; hydrogen; triethylamine; In methanol; acetone;
DOI:10.1002/chem.201003677

Reference yield:

: 1315281-46-9
p-bromoacetophenoneoctahydroroimatacene ester

: 20445-31-2
R-(+)-α-trifluoromethyl-α-methoxy-phenylacetic acid

: 1315281-48-1
C₆₈H₈₆BrF₉O₁₄

Guidance literature:: With dmap; 2,4,6-trichlorobenzoyl chloride; triethylamine; In toluene; at 0 - 20 ℃; for 4.25h; Inert atmosphere;
DOI:10.1002/chem.201003677