1-(3',5'-di(trifluoromethyl)phenyl)-2,3,4,5-tetramethylcyclopentadienyl titanium trichloride

Base Information

Chemical Name:1-(3',5'-di(trifluoromethyl)phenyl)-2,3,4,5-tetramethylcyclopentadienyl titanium trichloride
CAS No.:1015698-09-5
Molecular Formula:C₁₇H₁₅Cl₃F₆Ti
Molecular Weight:487.536
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(3',5'-di(trifluoromethyl)phenyl)-2,3,4,5-tetramethylcyclopentadienyl titanium trichloride

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Technology Process of 1-(3',5'-di(trifluoromethyl)phenyl)-2,3,4,5-tetramethylcyclopentadienyl titanium trichloride

There total 1 articles about 1-(3',5'-di(trifluoromethyl)phenyl)-2,3,4,5-tetramethylcyclopentadienyl titanium trichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.9%

: 1-(3',5'-di(trifluoromethyl)phenyl)-2,3,4,5-tetramethylcyclopentadiene

: 7550-45-0
titanium tetrachloride

: 1015698-09-5
1-(3',5'-di(trifluoromethyl)phenyl)-2,3,4,5-tetramethylcyclopentadienyl titanium trichloride

Guidance literature:: With CH₃CH₂CH₂CH₂Li; (CH₃)3SiCl; In toluene; (Ar); addn. of soln. of BuLi to cyclopentadiene deriv. in THF at -78°C, keeping at room temp. for 4 h, addn. of Me3SiCl in THF at -15°C, stirring for 2 h at room temp., evapn., extn. (toluene), addn. ofTiCl4 in toluene at -78°C; filtration, evapn., recrystn. (CH2Cl2/hexane (1:3)), elem. anal.;
DOI:10.1039/b921617k

Reference yield: 76.8%

: 72727-49-2
lithium 2,6-diisopropylphenolate

: 1015698-09-5
1-(3',5'-di(trifluoromethyl)phenyl)-2,3,4,5-tetramethylcyclopentadienyl titanium trichloride

: 1218922-84-9
1-(3',5'-di(trifluoromethyl)phenyl)-2,3,4,5-tetramethylcyclopentadienyl-TiCl₂(2,6-diisopropylphenolato)

Guidance literature:: In toluene; (Ar); addn. of toluene soln. of titanium compd. to toluene soln. of lithium phenolate deriv. at room temp., stirring at 80°C for 12 h; filtration, washing with toluene, evapn. of toluene soln., recrystn. (CH2Cl2/hexane (1:3)), elem. anal.;
DOI:10.1039/b921617k