ethyl N-phosphoryl-trans-4-aminocyclohexanecarboxylate

Base Information

Chemical Name:ethyl N-phosphoryl-trans-4-aminocyclohexanecarboxylate
CAS No.:117112-30-8
Molecular Formula:C₁₇H₃₂Cl₂N₃O₄P
Molecular Weight:444.339
Hs Code.:

ethyl N-<N'N'-di-(2-chloroethyl)amido-N''-morpholido>phosphoryl-trans-4-aminocyclohexanecarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl N-phosphoryl-trans-4-aminocyclohexanecarboxylate

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Technology Process of ethyl N-phosphoryl-trans-4-aminocyclohexanecarboxylate

There total 2 articles about ethyl N-phosphoryl-trans-4-aminocyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 110-91-8,99108-56-2
morpholine

: 117112-22-8
C₁₃H₂₄Cl₃N₂O₃P

: 117112-30-8,169811-11-4
ethyl N-phosphoryl-trans-4-aminocyclohexanecarboxylate

Guidance literature:: With triethylamine; In diethyl ether;
DOI:10.1007/BF00958340

Reference yield:

: 1678-68-8
ethyl trans-4-aminocyclohexanecarboxylate

: 117112-30-8,169811-11-4
ethyl N-phosphoryl-trans-4-aminocyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / 1.) 0 deg C, 1 h, 2.) ca.20 deg C, 2 h, 3.) 12 h

2: 40 percent / Et₃N / diethyl ether

With triethylamine; In diethyl ether;
DOI:10.1007/BF00958340