butyl-(2-butyl-1-methylene-buta-2,3-dienyl)-malonic acid

Base Information

• Chemical Name: butyl-(2-butyl-1-methylene-buta-2,3-dienyl)-malonic acid
• CAS No.: 101448-54-8
• Molecular Formula: C₁₆H₂₄O₄
• Molecular Weight: 280.364
• Mol file: 101448-54-8.mol

Synonyms:

Chemical Property of butyl-(2-butyl-1-methylene-buta-2,3-dienyl)-malonic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of butyl-(2-butyl-1-methylene-buta-2,3-dienyl)-malonic acid

There total 2 articles about butyl-(2-butyl-1-methylene-buta-2,3-dienyl)-malonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diethyl ether (60-29-7,927820-24-4) + 1-bromo-2-heptyne (18495-26-6) → oct-3-ynoic acid (57074-96-1) + 2-butyl-2,3-butadienoic acid (5665-73-6) + butyl-(2-butyl-1-methylene-buta-2,3-dienyl)-malonic acid (101448-54-8)

Guidance literature:

und anschliessend mit festem Kohlendioxid;

DOI:10.1021/jo01105a631 DOI:10.1021/jo01120a002 DOI:10.1021/ja01160a058

Reference yield:

methylammonium carbonate (15719-64-9,15719-76-3,97762-63-5) → oct-3-ynoic acid (57074-96-1) + butyl-(2-butyl-1-methylene-buta-2,3-dienyl)-malonic acid (101448-54-8)

Guidance literature:

With diethyl ether; anschliessend mit wss. Ammoniumchlorid-Loesung und mit wss. Salzsaeure;

DOI:10.1021/jo01120a002

upstream raw materials:

methylammonium carbonate

diethyl ether

1-bromo-2-heptyne