S-tosylsulfene chloride

Base Information

• Chemical Name: S-tosylsulfene chloride
• CAS No.: 145886-79-9
• Molecular Formula: C₇H₇ClO₂S₂
• Molecular Weight: 222.716

Synonyms:

Chemical Property of S-tosylsulfene chloride

Chemical Property:

Purity/Quality:

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Technology Process of S-tosylsulfene chloride

There total 1 articles about S-tosylsulfene chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

p-toluene sulfinic acid (536-57-2) → S-tosylsulfene chloride (145886-79-9)

Guidance literature:

With sulfur dichloride; triethylamine; In dichloromethane; Ambient temperature;

DOI:10.1007/BF00864549

Reference yield: 76.0%

S-tosylsulfene chloride (145886-79-9) + cyclohexene (110-83-8) → trans-2-chlorocyclohexyl-p-toluene thiosulfonate

Guidance literature:

In dichloromethane; for 13h; Ambient temperature;

DOI:10.1007/BF00864549

Reference yield:

1-hexene (592-41-6,25067-06-5) + S-tosylsulfene chloride (145886-79-9) → 1-chlorohexyl-2-p-toluene thiosulfonate + 2-chlorohexyl-1-p-toluene thiosulfonate

Guidance literature:

In dichloromethane; for 13h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;

DOI:10.1007/BF00864549

upstream raw materials:

p-toluene sulfinic acid

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