diethyl N-<4-benzoyl>-L-glutamate

Base Information

Chemical Name:diethyl N-<4-benzoyl>-L-glutamate
CAS No.:107716-29-0
Molecular Formula:C₁₈H₂₆N₂O₆
Molecular Weight:366.414
Hs Code.:

diethyl N-<4-<N-(hydroxyethyl)amino>benzoyl>-L-glutamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl N-<4-benzoyl>-L-glutamate

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Technology Process of diethyl N-<4-benzoyl>-L-glutamate

There total 1 articles about diethyl N-<4-benzoyl>-L-glutamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 75-21-8,99932-75-9
oxirane

: 13726-52-8
diethyl N-(p-aminobenzoyl)-L-glutamate

: 107716-29-0
diethyl N-<4-benzoyl>-L-glutamate

Guidance literature:: In acetic acid; 1.) 0 deg C, 2.) room temperature, 17 h;
DOI:10.1021/jm00119a012

Reference yield:

: 107716-29-0
diethyl N-<4-benzoyl>-L-glutamate

: 107716-41-6
N-<4-amino>ethyl>amino>benzoyl>-L-glutamic acid 5'-monophosphate

Guidance literature:: Multi-step reaction with 5 steps

1: 6.50 g / pyridine / 1 h / Ambient temperature

2: 18 percent / dimethylformamide / 48 h / 85 - 90 °C

3: 67 percent / HBr, phenol / acetic acid / 3.5 h

4: 41 percent / NaHCO₃ / dimethylformamide / 2 h / Ambient temperature

5: 1.) Zn, Cu, acetylacetone, 2.) NaOH / 1.) DMF, 50 deg C to 55 deg C, 1.5 h, 2.) ethanol, 48 h

With sodium hydroxide; hydrogen bromide; copper; sodium hydrogencarbonate; acetylacetone; zinc; phenol; In pyridine; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jm00119a012

Reference yield:

: 107716-29-0
diethyl N-<4-benzoyl>-L-glutamate

: 107716-37-0
diethyl N-<4-amino>ethyl>amino>benzoyl>-L-glutamate

Guidance literature:: Multi-step reaction with 4 steps

1: 6.50 g / pyridine / 1 h / Ambient temperature

2: 18 percent / dimethylformamide / 48 h / 85 - 90 °C

3: 67 percent / HBr, phenol / acetic acid / 3.5 h

4: 41 percent / NaHCO₃ / dimethylformamide / 2 h / Ambient temperature

With hydrogen bromide; sodium hydrogencarbonate; phenol; In pyridine; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jm00119a012