2-(2,2-Dimethoxyethyl)benzaldehyde

Base Information

Chemical Name:2-(2,2-Dimethoxyethyl)benzaldehyde
CAS No.:112396-12-0
Molecular Formula:C11H14O3
Molecular Weight:194.23
Hs Code.:
DSSTox Substance ID:DTXSID40551829
Wikidata:Q82431691

Synonyms:2-(2,2-dimethoxyethyl)benzaldehyde;112396-12-0;SCHEMBL10743250;DTXSID40551829;ZKTPVOMHZNFPPA-UHFFFAOYSA-N;2-(2,2-dimethoxyethyl) benzaldehyde

Suppliers and Price of 2-(2,2-Dimethoxyethyl)benzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2,2-Dimethoxyethyl)benzaldehyde

Chemical Property:

XLogP3:1.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:194.094294304
Heavy Atom Count:14
Complexity:166

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC(CC1=CC=CC=C1C=O)OC

Technology Process of 2-(2,2-Dimethoxyethyl)benzaldehyde

There total 4 articles about 2-(2,2-Dimethoxyethyl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2591-86-8
N-Formylpiperidine

: 112396-13-1
2-(2-bromophenyl)acetaldehyde dimethyl acetal

: 112396-12-0
Homophthalaldehyd-monodimethylacetal

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1) THF,hexane, -78 deg C, 1 h, 2) THF; hexane, from -78 deg C to r.t. during 12 h;
DOI:10.1002/jhet.5570240533

Reference yield:

: 130089-19-9,130089-23-5,59436-11-2
1-bromo-2-(2-methoxyethenyl)benzene

: 112396-12-0
Homophthalaldehyd-monodimethylacetal

Guidance literature:: Multi-step reaction with 2 steps

1: 93.2 percent / p-TsOH / 65 h / Heating

2: 1.) n-BuLi / 1.) THF, hexane, 30 min, -78 deg C, 2.a) THF, 1 h, -78 deg C, 2.b) room temperature

With n-butyllithium; toluene-4-sulfonic acid;
DOI:10.1002/ardp.19903230810

Reference yield:

: 6630-33-7
ortho-bromobenzaldehyde

: 112396-12-0
Homophthalaldehyd-monodimethylacetal

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) K-tert.-butylat / 1.) THF, -10 deg C, 2.a) -10 deg C, 2.b) 16 h, room temperature

2: 93.2 percent / p-TsOH / 65 h / Heating

3: 1.) n-BuLi / 1.) THF, hexane, 30 min, -78 deg C, 2.a) THF, 1 h, -78 deg C, 2.b) room temperature

With n-butyllithium; potassium tert-butylate; toluene-4-sulfonic acid;
DOI:10.1002/ardp.19903230810