C₂₇H₂₂ClF₄N₅O₃

Base Information

Chemical Name:C₂₇H₂₂ClF₄N₅O₃
CAS No.:1245941-00-7
Molecular Formula:C₂₇H₂₂ClF₄N₅O₃
Molecular Weight:575.95
Hs Code.:

C<sub>27</sub>H<sub>22</sub>ClF<sub>4</sub>N<sub>5</sub>O<sub>3</sub>

Synonyms:

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Chemical Property of C₂₇H₂₂ClF₄N₅O₃

Chemical Property:

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Technology Process of C₂₇H₂₂ClF₄N₅O₃

There total 4 articles about C₂₇H₂₂ClF₄N₅O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1245940-99-1
2-({[3-(4-Chlorophenyl)-4-(2-fluorobenzyl)-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]acetyl}amino)-2-[3-(trifluoromethyl)phenyl]propanamide

: 1245941-00-7
C₂₇H₂₂ClF₄N₅O₃

Guidance literature:: With silica gel; In 2-Methylpentane; ethyl acetate; Purification / work up; Resolution of racemate;

Reference yield:

: 349-76-8
3'-(trifluoromethyl)acetophenone

: 1245941-00-7
C₂₇H₂₂ClF₄N₅O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: ammonia; ammonium chloride / ethanol; water / 20 h / 70 °C / Autoclave

2.1: hydrogenchloride; water / 20 °C / Cooling with ice

3.1: benzotriazol-1-ol; N¹-((ethylimino)methylene)-N³,N³-dimethylpropane-1,3-diamine hydrochloride / N,N-dimethyl-formamide / 0.17 h / 20 °C

3.2: 20 h / 20 °C

4.1: silica gel / ethyl acetate; 2-Methylpentane / Resolution of racemate

With hydrogenchloride; N¹-((ethylimino)methylene)-N³,N³-dimethylpropane-1,3-diamine hydrochloride; ammonia; water; ammonium chloride; benzotriazol-1-ol; In ethanol; 2-Methylpentane; water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 1183104-54-2
2-amino-2-[3-(trifluoromethyl)phenyl]propanamide

: 1245941-00-7
C₂₇H₂₂ClF₄N₅O₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: benzotriazol-1-ol; N¹-((ethylimino)methylene)-N³,N³-dimethylpropane-1,3-diamine hydrochloride / N,N-dimethyl-formamide / 0.17 h / 20 °C

1.2: 20 h / 20 °C

2.1: silica gel / ethyl acetate; 2-Methylpentane / Resolution of racemate

With N¹-((ethylimino)methylene)-N³,N³-dimethylpropane-1,3-diamine hydrochloride; benzotriazol-1-ol; In 2-Methylpentane; ethyl acetate; N,N-dimethyl-formamide;