Ni(P(C₆H₅)2)*(PH(C₆H₅)2)

Base Information

Chemical Name:Ni(P(C₆H₅)2)*(PH(C₆H₅)2)
CAS No.:133952-91-7
Molecular Formula:C₁₂H₁₀NiP*C₁₂H₁₁P
Molecular Weight:430.068
Hs Code.:

Ni(P(C<sub>6</sub>H<sub>5</sub>)2)*(PH(C<sub>6</sub>H<sub>5</sub>)2)

Synonyms:

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Chemical Property of Ni(P(C₆H₅)2)*(PH(C₆H₅)2)

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Technology Process of Ni(P(C₆H₅)2)*(PH(C₆H₅)2)

There total 1 articles about Ni(P(C₆H₅)2)*(PH(C₆H₅)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7440-02-0
nickel

: 829-85-6
diphenylphosphane

: 133952-91-7
Ni(P(C₆H₅)2)*(PH(C₆H₅)2)

Guidance literature:: In acetonitrile; Electrolysis; under N2; the electrolysis was performed in a cell containing platinum as cathode and nickel as anode at 20 V and 50 mA for 1.25 h; electrolyte: tetraethylammonium perchlorate;; the crystalline material which deposited throughout the electrolysis was collected and washed with cold acetonitrile and dried; elem. anal.;;
DOI:10.1039/DT9910000011

Reference yield: 90.0%

: 10544-50-0
sulfur

: 133952-91-7
Ni(P(C₆H₅)2)*(PH(C₆H₅)2)

: Ni(dtpi)2

Guidance literature:: In benzene; byproducts: H2S; under N2; stirring overnight;; filtn.; deposited crystals were collected, washed with with toluene and dried in vacuo;;
DOI:10.1039/DT9910000011

Reference yield: 67.0%

: 133952-91-7
Ni(P(C₆H₅)2)*(PH(C₆H₅)2)

: 103-72-0
phenyl isothiocyanate

: 134023-87-3
{Ni(P(C₆H₅)2(SNCC₆H₅))2}

Guidance literature:: In dichloromethane; Ni(PPh2)2PPh2H was added to the soln. of PhNCS at room temp.; the soln. was left for 24 h;; the volume was reduced to 5 ml; addn. of acetonitrile; the precipitated crystals were collected, washed with acetonitrile and dried; elem. anal.;
DOI:10.1039/DT9910000011