Technology Process of C25H34N2O5
There total 3 articles about C25H34N2O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: N,N-dimethyl-formamide; mineral oil / 0.33 h / 20 °C / Inert atmosphere
1.2: 7 h
2.1: ethanol / 0.5 h / 100 °C / 12929 Torr / MW reactor
3.1: hydrogen; acetic acid / palladium 10% on activated carbon / water; methanol / 5 h / 2585.81 Torr
3.2: 1 h / 20 °C
4.1: triethylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / dichloromethane / 20 °C
With
hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; acetic acid; triethylamine;
palladium 10% on activated carbon;
In
methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: ethanol / 0.5 h / 100 °C / 12929 Torr / MW reactor
2.1: hydrogen; acetic acid / palladium 10% on activated carbon / water; methanol / 5 h / 2585.81 Torr
2.2: 1 h / 20 °C
3.1: triethylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / dichloromethane / 20 °C
With
hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; acetic acid; triethylamine;
palladium 10% on activated carbon;
In
methanol; ethanol; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: hydrogen; acetic acid / palladium 10% on activated carbon / water; methanol / 5 h / 2585.81 Torr
1.2: 1 h / 20 °C
2.1: triethylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / dichloromethane / 20 °C
With
hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; acetic acid; triethylamine;
palladium 10% on activated carbon;
In
methanol; dichloromethane; water;