4-(α-Methyl-benzyl)-2-methyl-thiosemicarbazid

Base Information

• Chemical Name: 4-(α-Methyl-benzyl)-2-methyl-thiosemicarbazid
• CAS No.: 4312-18-9
• Molecular Formula: C₁₀H₁₅N₃S
• Molecular Weight: 209.315
• Mol file: 4312-18-9.mol

Synonyms:

Chemical Property of 4-(α-Methyl-benzyl)-2-methyl-thiosemicarbazid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-(α-Methyl-benzyl)-2-methyl-thiosemicarbazid

There total 2 articles about 4-(α-Methyl-benzyl)-2-methyl-thiosemicarbazid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1-isothiocyanato-ethyl)-benzene (24277-44-9,32393-32-1,24277-43-8,4478-92-6) + methylhydrazine (60-34-4) → 4-(α-Methyl-benzyl)-2-methyl-thiosemicarbazid (4312-18-9)

Guidance literature:

In diethyl ether;

Reference yield:

→ 4-(α-Methyl-benzyl)-2-methyl-thiosemicarbazid (4312-18-9)

Guidance literature:

α-Methyl-benzyl-isothiocyanat, Methylhydrazin;

Reference yield: 57.0%

potassium tetrachloropalladate(II) (10025-98-6) + 4-(α-Methyl-benzyl)-2-methyl-thiosemicarbazid (4312-18-9) → Pd{C6H5CH(CH3)NHC(S)N(CH3)NH2}2Cl(1+)*Cl(1-)*3H2O = Pd{C6H5CH(CH3)NHC(S)N(CH3)NH2}2Cl2*3H2O

Guidance literature:

In ethanol; water; mixed; heated to 40-50°C; pH=1-2 (HCl); ppt. sepd.; washed (ether/water); recrystd. (ethanol/water); dried (vac., CaCl2, 75°C); elem. anal.;

upstream raw materials:

(1-isothiocyanato-ethyl)-benzene

methylhydrazine