TcCl(CO)2(P(CH₃)2C₆H₅)3

Base Information

Chemical Name:TcCl(CO)2(P(CH₃)2C₆H₅)3
CAS No.:64347-48-4
Molecular Formula:C₂₆H₃₃ClO₂P₃Tc
Molecular Weight:603.828
Hs Code.:

TcCl(CO)2(P(CH<sub>3</sub>)2C<sub>6</sub>H<sub>5</sub>)3

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Chemical Property of TcCl(CO)2(P(CH₃)2C₆H₅)3

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Technology Process of TcCl(CO)2(P(CH₃)2C₆H₅)3

There total 2 articles about TcCl(CO)2(P(CH₃)2C₆H₅)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 88979-87-7
mer-[trichlorotris(dimethylphenylphosphine)-technetium(III)]

: 77698-71-6,64347-48-4
TcCl(CO)2(P(CH₃)2C₆H₅)3

Guidance literature:: With CO; In toluene; reacting Tc complex with CO; stirring with toluene and P(CH3)2C6H5 (excess), room temp., 6h; concentrating; addn. of pentane; crystn.;

Reference yield:

: 88979-87-7
mer-[trichlorotris(dimethylphenylphosphine)-technetium(III)]

: 201230-82-2
carbon monoxide

: 672-66-2
Dimethyl(phenyl)phosphine

: 64347-48-4,77698-71-6
cis-{TcCl(CO)2(P(CH₃)2C₆H₅)3}

Guidance literature:: In 1,2-dimethoxyethane; boiling;
DOI:10.1016/S0022-328X(00)80858-X

Reference yield: 85.0%

: 77698-71-6,64347-48-4
TcCl(CO)2(P(CH₃)2C₆H₅)3

: 785-86-4,813445-46-4
1,3-di(p-tolyl)triaz-1-ene

: 99354-91-3
[Tc(P(CH₃)2C₆H₅)2(CO)2(CH₃C₆H₄N₃C₆H₄CH₃)]

Guidance literature:: With n-butyllithium; In benzene; addn. of n-butyllithium soln. (hexane) to ligand soln. (benzene) under N2, room temp.; addn. of solid Tc complex; boiling a few min; refluxing under N2, 3h; concentrating to a third of its volume; filtration; addn. of ethanol; pptn.; washing solid (H2O, ethanol, diethylether); crystn. (CH2Cl2/ethanol 7/3v/v); elem. anal.;