Ru(C₆(CH₃)6)(PH(C₆H₁₁)2)Cl₂

Base Information

Chemical Name:Ru(C₆(CH₃)6)(PH(C₆H₁₁)2)Cl₂
CAS No.:89770-65-0
Molecular Formula:C₂₄H₄₁Cl₂PRu
Molecular Weight:532.539
Hs Code.:

Ru(C<sub>6</sub>(CH<sub>3</sub>)6)(PH(C<sub>6</sub>H<sub>11</sub>)2)Cl<sub>2</sub>

Synonyms:

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Chemical Property of Ru(C₆(CH₃)6)(PH(C₆H₁₁)2)Cl₂

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Technology Process of Ru(C₆(CH₃)6)(PH(C₆H₁₁)2)Cl₂

There total 1 articles about Ru(C₆(CH₃)6)(PH(C₆H₁₁)2)Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: [RuCl₂(hexamethylbenzene)]2

: 829-84-5
dicyclohexylphosphane

: 89770-65-0
Ru(C₆(CH₃)6)(PH(C₆H₁₁)2)Cl₂

Guidance literature:: In dichloromethane; Ru complex treated with 2 mol PHCy2 in CH2Cl2 at 22°C under N2 for 24 h; pptn.; elem. anal.;
DOI:10.1016/S0022-328X(00)98703-5

Reference yield: 90.0%

: 89770-65-0
Ru(C₆(CH₃)6)(PH(C₆H₁₁)2)Cl₂

: 22722-98-1
sodium bis(2-methoxyethoxy)aluminium dihydride

: 89770-64-9
Ru(C₆(CH₃)6)(PH(C₆H₁₁)2)H₂

Guidance literature:: In tetrahydrofuran; Ru complex dissolved in dry THF, reduced at 22°C with 2 equiv. of Na(AlH2(OCH2CH2OMe)2); filtration through alumina (activity I); elem. anal.;
DOI:10.1016/S0022-328X(00)98703-5

Reference yield:

: 89770-65-0
Ru(C₆(CH₃)6)(PH(C₆H₁₁)2)Cl₂

: 22722-98-1
sodium bis(2-methoxyethoxy)aluminium dihydride

: 89770-66-1
Ru(C₆(CH₃)6)(PH(C₆H₁₁)2)HCl

Guidance literature:: In tetrahydrofuran; Ru complex dissolved in dry THF, reduced at 22°C with 1 equiv. of Na(AlH2(OCH2CH2OMe)2); not isolated; detected by NMR;
DOI:10.1016/S0022-328X(00)98703-5