3-cholesteryl p-isocyanobenzoate

Base Information

Chemical Name:3-cholesteryl p-isocyanobenzoate
CAS No.:131809-14-8
Molecular Formula:C₃₅H₄₉NO₂
Molecular Weight:515.78
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-cholesteryl p-isocyanobenzoate

Chemical Property:

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Technology Process of 3-cholesteryl p-isocyanobenzoate

There total 5 articles about 3-cholesteryl p-isocyanobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.1%

: 132042-72-9
3-cholesteryl p-formamidobenzoate

: 131809-14-8
3-cholesteryl p-isocyanobenzoate

Guidance literature:: With triethylamine; trichloromethyl chloroformate; In dichloromethane;

Reference yield:

: 57-88-5
cholesterol

: 131809-14-8
3-cholesteryl p-isocyanobenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 78.7 percent / pyridine / tetrahydrofuran / 96 h / Ambient temperature

2: 82.3 percent / H₂ / 10percent palladium on charcoal / tetrahydrofuran / 84 h / 760 Torr

3: 60.3 percent / acetic acid / CH₂Cl₂ / 1.5 h / ice-water bath

4: 42.1 percent / trichloromethyl chlorocarbonate, triethylamine / CH₂Cl₂

With pyridine; hydrogen; acetic acid; triethylamine; trichloromethyl chloroformate; palladium on activated charcoal; In tetrahydrofuran; dichloromethane;

Reference yield:

: 23838-12-2
cholesteryl 4-nitrobenzoate

: 131809-14-8
3-cholesteryl p-isocyanobenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 82.3 percent / H₂ / 10percent palladium on charcoal / tetrahydrofuran / 84 h / 760 Torr

2: 60.3 percent / acetic acid / CH₂Cl₂ / 1.5 h / ice-water bath

3: 42.1 percent / trichloromethyl chlorocarbonate, triethylamine / CH₂Cl₂

With hydrogen; acetic acid; triethylamine; trichloromethyl chloroformate; palladium on activated charcoal; In tetrahydrofuran; dichloromethane;