carbonyl>amino>-2-cyclooctene

Base Information

Chemical Name:carbonyl>amino>-2-cyclooctene
CAS No.:132646-19-6
Molecular Formula:C₂₁H₂₉NO₂
Molecular Weight:327.467
Hs Code.:

<N-<<(trans-2-phenylcyclohexyl)oxy>carbonyl>amino>-2-cyclooctene

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of carbonyl>amino>-2-cyclooctene

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Technology Process of carbonyl>amino>-2-cyclooctene

There total 4 articles about carbonyl>amino>-2-cyclooctene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₄H₃₇NO₃SSi

: 132646-19-6,132746-38-4
carbonyl>amino>-2-cyclooctene

Guidance literature:: With lithium hydroxide; water; In tetrahydrofuran; methanol; for 3h; Yield given; Ambient temperature;
DOI:10.1021/ja00009a045

Reference yield:

: 129966-10-5
(S)-trans-2-phenylcyclohexyl carbamate

: 132646-19-6,132746-38-4
carbonyl>amino>-2-cyclooctene

Guidance literature:: Multi-step reaction with 4 steps

1: SOCl₂, pyridine / benzene / 14.25 h / Ambient temperature

2: SnCl₄ / CH₂Cl₂ / 0.33 h / -78 °C

3: 1,2-dichloro-ethane / 1.) RT, 90 min, 2.) 50 deg C, 90 min, 3.) reflux, overnight

4: LiOH, H₂O / tetrahydrofuran; methanol / 3 h / Ambient temperature

With pyridine; lithium hydroxide; thionyl chloride; water; tin(IV) chloride; In tetrahydrofuran; methanol; dichloromethane; 1,2-dichloro-ethane; benzene;
DOI:10.1021/ja00009a045

Reference yield:

: 107575-41-7,130060-02-5
(S)-trans-2-phenylcyclohexyl N-sulfinylcarbamate

: 132646-19-6,132746-38-4
carbonyl>amino>-2-cyclooctene

Guidance literature:: Multi-step reaction with 3 steps

1: SnCl₄ / CH₂Cl₂ / 0.33 h / -78 °C

2: 1,2-dichloro-ethane / 1.) RT, 90 min, 2.) 50 deg C, 90 min, 3.) reflux, overnight

3: LiOH, H₂O / tetrahydrofuran; methanol / 3 h / Ambient temperature

With lithium hydroxide; water; tin(IV) chloride; In tetrahydrofuran; methanol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/ja00009a045