[1-S-2-Ph-1,2-closo-C₂B₁₀H₁₀]2

Base Information

Chemical Name:[1-S-2-Ph-1,2-closo-C₂B₁₀H₁₀]2
CAS No.:17525-40-5
Molecular Formula:C₁₆H₃₀B₂₀S₂
Molecular Weight:502.766
Hs Code.:

[1-S-2-Ph-1,2-closo-C<sub>2</sub>B<sub>10</sub>H<sub>10</sub>]2

Synonyms:

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Chemical Property of [1-S-2-Ph-1,2-closo-C₂B₁₀H₁₀]2

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Technology Process of [1-S-2-Ph-1,2-closo-C₂B₁₀H₁₀]2

There total 1 articles about [1-S-2-Ph-1,2-closo-C₂B₁₀H₁₀]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 17522-85-9
1-mercapto-2-phenyl-ortho-carborane

: 17525-40-5
[1-S-2-Ph-1,2-closo-C₂B₁₀H₁₀]2

Guidance literature:: With KOH; iodine; In ethanol; under N2; carborane added to soln. of KOH in deoxygenated ethanol, mixt.stirred for 10 min, soln. of I2 added dropwise, mixt. stirred for 10 mi n; evapd., water added to residue, extd. with diethyl ether, org. layer sepd. and washed with water, dried over MgSO4, evapd. under vac., residue recrystd. from warm petroleum ether; elem. anal.;
DOI:10.1039/b502328a

Reference yield: 74.0%

: 17525-40-5
[1-S-2-Ph-1,2-closo-C₂B₁₀H₁₀]2

: 1112-67-0
tetrabutyl-ammonium chloride

: 7732-18-5
water

: [NBu₄]2[7-S-8-Ph-7,8-nido-C₂B₉H₁₀]2*4H₂O

Guidance literature:: With piperidine; In ethanol; under N2; excess of piperidine added to soln. of carborane in degassed abs. ethanol, mixt. refluxed for 9 h, evapd. under vac., excess of N(C4H9)4Cl in water added to residue; solid filtered off, washed with water and diethyl ether, dried under vac.; elem. anal.;
DOI:10.1039/b502328a

Reference yield: 73.0%

: 17525-40-5
[1-S-2-Ph-1,2-closo-C₂B₁₀H₁₀]2

: 75-57-0
tetramethlyammonium chloride

: 856255-17-9
[NMe₄][1-S-2-Ph-1,2-closo-C₂B₁₀H₁₀]

Guidance literature:: With KOH; In ethanol; under N2; carborane added to soln. of KOH in degassed abs. ethanol, mixt. refluxed for 3 h, cooled to room temp., evapd. under vac., water and aq. N(CH3)4Cl successively added to residue; solid filtered off, washed with water and diethyl ether; elem. anal.;
DOI:10.1039/b502328a