[Zn(2,2'-bipyridine)(N,N'-bis(salicylidenato)-p-phenylenediamine)]2*hexafluorobenzene

Base Information

• Chemical Name: [Zn(2,2'-bipyridine)(N,N'-bis(salicylidenato)-p-phenylenediamine)]2*hexafluorobenzene
• CAS No.: 1007843-98-2
• Molecular Formula: C₆F₆*C₆₀H₄₄N₈O₄Zn₂
• Molecular Weight: 1257.9
• Mol file: 1007843-98-2.mol

Synonyms:

Chemical Property of [Zn(2,2'-bipyridine)(N,N'-bis(salicylidenato)-p-phenylenediamine)]2*hexafluorobenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [Zn(2,2'-bipyridine)(N,N'-bis(salicylidenato)-p-phenylenediamine)]2*hexafluorobenzene

There total 1 articles about [Zn(2,2'-bipyridine)(N,N'-bis(salicylidenato)-p-phenylenediamine)]2*hexafluorobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

Hexafluorobenzene (392-56-3) + [zinc(II)(2,2'-bipyridine)(N,N'-bis(salicylidene)-p-phenylenediamine)]2 (791845-30-2) → [Zn(2,2'-bipyridine)(N,N'-bis(salicylidenato)-p-phenylenediamine)]2*hexafluorobenzene (1007843-98-2)

Guidance literature:

With NH₄PF₆; In methanol; water; dimethyl sulfoxide; F-compd. in MeOH was dropwise added to DMSO soln. of metal-compd., stirring for 4 h, cooling in a fridge for 24 h, aq. NH4PF6 was added; solid was filtered off, washed with MeOH followed by Et2O, dissoln. in DMSO, MeOH was added, solid was dried in vac., elem. anal.;

DOI:10.1016/j.poly.2007.09.017

upstream raw materials:

Hexafluorobenzene

[zinc(II)(2,2'-bipyridine)(N,N'-bis(salicylidene)-p-phenylenediamine)]2