(2E,4E,6E)-(R)-8-[(2S,3S)-2-(tert-Butyl-diphenyl-silanyloxy)-3-methyl-pentanoyloxy]-8-((R)-2-methyl-oxiranyl)-octa-2,4,6-trienoic acid methyl ester

Base Information

Chemical Name:(2E,4E,6E)-(R)-8-[(2S,3S)-2-(tert-Butyl-diphenyl-silanyloxy)-3-methyl-pentanoyloxy]-8-((R)-2-methyl-oxiranyl)-octa-2,4,6-trienoic acid methyl ester
CAS No.:114029-77-5
Molecular Formula:C₃₄H₄₄O₆Si
Molecular Weight:576.805
Hs Code.:

(2E,4E,6E)-(R)-8-[(2S,3S)-2-(tert-Butyl-diphenyl-silanyloxy)-3-methyl-pentanoyloxy]-8-((R)-2-methyl-oxiranyl)-octa-2,4,6-trienoic acid methyl ester

Synonyms:

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Chemical Property of (2E,4E,6E)-(R)-8-[(2S,3S)-2-(tert-Butyl-diphenyl-silanyloxy)-3-methyl-pentanoyloxy]-8-((R)-2-methyl-oxiranyl)-octa-2,4,6-trienoic acid methyl ester

Chemical Property:

Purity/Quality:

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Technology Process of (2E,4E,6E)-(R)-8-[(2S,3S)-2-(tert-Butyl-diphenyl-silanyloxy)-3-methyl-pentanoyloxy]-8-((R)-2-methyl-oxiranyl)-octa-2,4,6-trienoic acid methyl ester

There total 55 articles about (2E,4E,6E)-(R)-8-[(2S,3S)-2-(tert-Butyl-diphenyl-silanyloxy)-3-methyl-pentanoyloxy]-8-((R)-2-methyl-oxiranyl)-octa-2,4,6-trienoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73-32-5,959215-79-3,18875-42-8
L-isoleucine

: 104855-42-7,105015-88-1,114029-77-5,139164-21-9,139164-22-0
Methyl (9S),10-Epoxy-(8R)-((2'S)-tert-butyldiphenylsilyloxy-(3'S)-methylpentanoyloxy)-9-methyl-deca-(E,E,E)-trienoate

Guidance literature:: Multi-step reaction with 6 steps

1: sodium nitrite

2: p-toluenesulphonic acid

3: lithium carbonate, water / methanol

4: imidazole / dimethylformamide

5: H₂ / palladium on carbon / ethanol

6: dicyclohexylcarbodiimide, 4-pyrrolidinopyridine / CH₂Cl₂

With 1H-imidazole; water; hydrogen; lithium carbonate; 4-pyrrolidin-1-ylpyridine; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; sodium nitrite; palladium on activated charcoal; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1248/cpb.34.2668

Reference yield:

: 104973-58-2
(2S,3S)-2-(acetyloxy)-3-methylpentanoic acid

: 104855-42-7,105015-88-1,114029-77-5,139164-21-9,139164-22-0
Methyl (9S),10-Epoxy-(8R)-((2'S)-tert-butyldiphenylsilyloxy-(3'S)-methylpentanoyloxy)-9-methyl-deca-(E,E,E)-trienoate

Guidance literature:: Multi-step reaction with 5 steps

1: p-toluenesulphonic acid

2: lithium carbonate, water / methanol

3: imidazole / dimethylformamide

4: H₂ / palladium on carbon / ethanol

5: dicyclohexylcarbodiimide, 4-pyrrolidinopyridine / CH₂Cl₂

With 1H-imidazole; water; hydrogen; lithium carbonate; 4-pyrrolidin-1-ylpyridine; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1248/cpb.34.2668

Reference yield:

: 104855-40-5
benzyl (2S,3S)-2-acetoxy-3-methylpentanoate

: 104855-42-7,105015-88-1,114029-77-5,139164-21-9,139164-22-0
Methyl (9S),10-Epoxy-(8R)-((2'S)-tert-butyldiphenylsilyloxy-(3'S)-methylpentanoyloxy)-9-methyl-deca-(E,E,E)-trienoate

Guidance literature:: Multi-step reaction with 4 steps

1: lithium carbonate, water / methanol

2: imidazole / dimethylformamide

3: H₂ / palladium on carbon / ethanol

4: dicyclohexylcarbodiimide, 4-pyrrolidinopyridine / CH₂Cl₂

With 1H-imidazole; water; hydrogen; lithium carbonate; 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1248/cpb.34.2668