{PdCl₂(Se₂(C₆H₅)2)}2

Base Information

• Chemical Name: {PdCl₂(Se₂(C₆H₅)2)}2
• CAS No.: 127416-20-0
• Molecular Formula: C₂₄H₂₀Cl₄Pd₂Se₄
• Molecular Weight: 978.915
• Mol file: 127416-20-0.mol

Synonyms:

Chemical Property of {PdCl₂(Se₂(C₆H₅)2)}2

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of {PdCl₂(Se₂(C₆H₅)2)}2

There total 2 articles about {PdCl₂(Se₂(C₆H₅)2)}2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

bis(benzonitrile)palladium(II) dichloride + diphenyl diselenide (1666-13-3) → {PdCl2(Se2(C6H5)2)}2 (127416-20-0)

Guidance literature:

In benzene; react. under dry N2, addn. of Ar2Se2 to the Pd complex in benzene at room temp., stirring for 4 h; filtration, washing with benzene and ether, drying in vac., elem. anal.;

DOI:10.1016/S0020-1693(00)80811-7

Reference yield: 84.0%

sodium tetrachloropalladate(II) + diphenyl diselenide (1666-13-3) → {PdCl2(Se2(C6H5)2)}2 (127416-20-0)

Guidance literature:

In ethanol; react. under dry N2, addn. of Ar2Se2 in EtOH to the Pd complex in EtOH, stirring for 2 h, pptn.; washing with ice-cold water, cold alcohol and ether, drying in vac. ,elem. anal.;

DOI:10.1016/S0020-1693(00)80811-7

Reference yield:

{PdCl2(Se2(C6H5)2)}2 (127416-20-0) → phenylselenol palladium(II) Cl (127441-30-9)

Guidance literature:

In methanol; ethanol; refluxing in methanol/ethanol; successive washings with methanol/ethanol and CHCl3;

DOI:10.1016/S0020-1693(00)80811-7

upstream raw materials:

diphenyl diselenide

Downstream raw materials:

phenylselenol palladium(II) Cl