Sb(2,4,6-Me₃C₆H₂)3BrOH

Base Information

Chemical Name:Sb(2,4,6-Me₃C₆H₂)3BrOH
CAS No.:198917-88-3
Molecular Formula:C₂₇H₃₄BrOSb
Molecular Weight:576.22
Hs Code.:

Sb(2,4,6-Me<sub>3</sub>C<sub>6</sub>H<sub>2</sub>)3BrOH

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Chemical Property of Sb(2,4,6-Me₃C₆H₂)3BrOH

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Technology Process of Sb(2,4,6-Me₃C₆H₂)3BrOH

There total 3 articles about Sb(2,4,6-Me₃C₆H₂)3BrOH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 106870-60-4
trimesitylantimony dibromide

: 7732-18-5
water

: 1310-73-2
sodium hydroxide

: 198917-88-3
Sb(2,4,6-Me₃C₆H₂)3BrOH

Guidance literature:: In methanol; water; inert atmosphere; addn. of slight excess of concd. aq. NaOH to Sb-compd.soln. (in MeOH), refluxing for 20 h; solvent removal (vac.), dissoln. in CH2Cl2, filtration, evapn., recrystn. (CHCl3/hexane); elem. anal.;
DOI:10.1016/S0022-328X(97)00208-8

Reference yield:

: 576-83-0
2,4,6-trimethylphenyl bromide

: 198917-88-3
Sb(2,4,6-Me₃C₆H₂)3BrOH

Guidance literature:: Multi-step reaction with 3 steps

1: Li / diethyl ether

2: dichloromethane

3: water; methanol

With Li; In methanol; diethyl ether; dichloromethane; water;
DOI:10.1016/S0022-328X(97)00208-8

Reference yield:

: 23822-17-5
tris(2,4,6-trimethylphenyl)antimony

: 198917-88-3
Sb(2,4,6-Me₃C₆H₂)3BrOH

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane

2: water; methanol

In methanol; dichloromethane; water;
DOI:10.1016/S0022-328X(97)00208-8