tris(2,4,6-trimethylphenyl)antimony

Base Information

Chemical Name:tris(2,4,6-trimethylphenyl)antimony
CAS No.:23822-17-5
Molecular Formula:C₂₇H₃₃Sb
Molecular Weight:479.309
Hs Code.:

Synonyms:tris(2,4,6-trimethylphenyl)antimony

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Chemical Property of tris(2,4,6-trimethylphenyl)antimony

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Technology Process of tris(2,4,6-trimethylphenyl)antimony

There total 3 articles about tris(2,4,6-trimethylphenyl)antimony which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 576-83-0
2,4,6-trimethylphenyl bromide

: 10025-91-9
antimony(III) chloride

: 23822-17-5
tris(2,4,6-trimethylphenyl)antimony

Guidance literature:: 2,4,6-trimethylphenyl bromide; With iodine; magnesium; In tetrahydrofuran; for 2h; Inert atmosphere; Reflux;

antimony(III) chloride; In tetrahydrofuran; diethyl ether; for 2h; Inert atmosphere; Reflux;
DOI:10.1002/chem.201500281

Reference yield:

: 10025-91-9
antimony(III) chloride

: 2633-66-1
2-mesitylmagnesium bromide

: 23822-17-5
tris(2,4,6-trimethylphenyl)antimony

Guidance literature:: With 1,2-dibromethane; (Ar); Grignard reaction according to C.Ludwig, H.-J.Goetze, Spectrochim.Acta Part A 51A(1995)2019, P.Pfeiffer, Ber. Dtsch. Chem. Ges. 37(1904)4 620 or F.F.Blicke, U.O.Oakdale, F.D.Smith, J. Am. Soc. 53(1931)1025;
DOI:10.1016/S1386-1425(97)00176-5