N₂-diisobutylboryl-N₁-isopropylbenzamidine

Base Information

Chemical Name:N₂-diisobutylboryl-N₁-isopropylbenzamidine
CAS No.:74333-42-9
Molecular Formula:C₁₈H₃₁BN₂
Molecular Weight:286.269
Hs Code.:

N<sub>2</sub>-diisobutylboryl-N<sub>1</sub>-isopropylbenzamidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N₂-diisobutylboryl-N₁-isopropylbenzamidine

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Technology Process of N₂-diisobutylboryl-N₁-isopropylbenzamidine

There total 1 articles about N₂-diisobutylboryl-N₁-isopropylbenzamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1116-39-8
triisobutylborane

: 53510-31-9
N-(isopropyl)benzimidamide

: 74333-42-9
N₂-diisobutylboryl-N₁-isopropylbenzamidine

Guidance literature:: In tetrahydrofuran; byproducts: CH(CH3)3; (Ar); mixt. of N-isopropylbenzamidine and triisobutylborane refluxed until gas evolution ceased (3-8 h); solvent removed under vac.; distd. in vac.; IR; NMR; elem. anal.;
DOI:10.1007/BF00949640

Reference yield:

: 74333-42-9
N₂-diisobutylboryl-N₁-isopropylbenzamidine

: 74323-72-1
[NB(CH₂CH(CH₃)2)2C(C₆H₅)NH(CH(CH₃)2)]2

Guidance literature:: In neat (no solvent); stored under Ar for a period from 3 days to 3 months; crystals treated with methanol and filtered; then crystals washed with methanol; MS; IR; elem. anal.;
DOI:10.1007/BF00949640