E-α-deutero-β-trimethylstannylstyrene

Base Information

Chemical Name:E-α-deutero-β-trimethylstannylstyrene
CAS No.:82318-99-8
Molecular Formula:C₁₁H₁₆Sn
Molecular Weight:267.95
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of E-α-deutero-β-trimethylstannylstyrene

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Technology Process of E-α-deutero-β-trimethylstannylstyrene

There total 2 articles about E-α-deutero-β-trimethylstannylstyrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 62359-30-2
trimethyltin hydride

: 536-74-3
phenylacetylene

: 82319-00-4,82318-99-8
Z-α-deutero-β-trimethylstannylstyrene

: 82319-00-4,82318-99-8
E-α-deutero-β-trimethylstannylstyrene

Guidance literature:: In neat (no solvent); Irradiation (UV/VIS); a mixt. of Sn(CH3)3(2)H and phenylacetylene under N2 was irradiated for4 h; distd.;

Reference yield:

: 62359-30-2
trimethyltin hydride

: 536-74-3
phenylacetylene

: 82319-00-4,82318-99-8
Z-α-deutero-β-trimethylstannylstyrene

: 82319-00-4,82318-99-8
E-α-deutero-β-trimethylstannylstyrene

Guidance literature:: In neat (no solvent); Irradiation (UV/VIS); a mixt. of Sn(CH3)3(2)H and phenylacetylene under N2 was irradiated for4 h; distd.;

Reference yield:

: 82318-99-8,82319-00-4
Sn(CH₃)3CHC⁽²⁾HC₆H₅

: 513-81-5
2,3-dimethyl-buta-1,3-diene

: (CH₃)3SnCHC⁽²⁾HC₆H₅CH₂C(CH₃)C(CH₃)CH₂

: (CH₃)3SnCHC⁽²⁾HC₆H₅CH₂C(CH₃)C(CH₃)CH₂

Guidance literature:: In neat (no solvent); Sn deriv. heating in a slight excess of the butadiene in a sealed tube for 63 h at 180°C to give a mixt. of E,Z-isomers (80:20) in a total yield 30%; isolated by gas chromy. at 180°C; identified by NMR and mass spectra;
DOI:10.1016/S0022-328X(00)85701-0