(S)-2-(dimethylamino)-3-(1H-4-imidazolyl)propanoic acid

Base Information

Chemical Name:(S)-2-(dimethylamino)-3-(1H-4-imidazolyl)propanoic acid
CAS No.:58147-58-3
Molecular Formula:C₈H₁₃N₃O₂
Molecular Weight:183.21
Hs Code.:

Synonyms:

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Chemical Property of (S)-2-(dimethylamino)-3-(1H-4-imidazolyl)propanoic acid

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Technology Process of (S)-2-(dimethylamino)-3-(1H-4-imidazolyl)propanoic acid

There total 2 articles about (S)-2-(dimethylamino)-3-(1H-4-imidazolyl)propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 71-00-1
L-histidine

: 24940-57-6,58147-58-3
(S)-2-(dimethylamino)-3-(1H-4-imidazolyl)propanoic acid

Guidance literature:: With sodium cyanoborohydride; acetic acid; In water; acetonitrile; at 21 ℃; for 1h; pH=Ca.7; Inert atmosphere;
DOI:10.1021/acs.joc.7b03187

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 645-35-2
L-histidine monohydrochloride

: 24940-57-6,58147-58-3
(S)-2-(dimethylamino)-3-(1H-4-imidazolyl)propanoic acid

Guidance literature:: With palladium on activated charcoal; hydrogen; In water; for 0.833333h; under 9000.9 Torr;
DOI:10.1021/acs.jnatprod.5b00942

Reference yield: 20.0%

: 24940-57-6,58147-58-3
(S)-2-(dimethylamino)-3-(1H-4-imidazolyl)propanoic acid

: 3-hydroxy-2-((((9Z,12Z)-octadeca-9,12-dienoyl)oxy)methyl)propyl 3,5-di-tert-butylbenzoate

: 3-((Nα,Nα-dimethyl-L-histidyl)oxy)-2-((((9Z,12Z)-octadeca-9,12-dienoyl)oxy)methyl)propyl 3,5-di-tert-butylbenzoate

Guidance literature:: With dmap; N-ethyl-N,N-diisopropylamine; ((3H-[1,2,3]triazolo[4,5-b]pyridin-3-yl)oxy)tri(pyrrolidin-1-yl)phosphonium hexafluorophosphate(V); In N,N-dimethyl-formamide; at 23 ℃; for 18h; Inert atmosphere;