2-Ethoxy-4-nitrobenzaldehyde

Base Information

Chemical Name:2-Ethoxy-4-nitrobenzaldehyde
CAS No.:1134-43-6
Molecular Formula:C9H9NO4
Molecular Weight:195.175
Hs Code.:
DSSTox Substance ID:DTXSID20599688
Wikidata:Q82495609
Mol file:1134-43-6.mol

Synonyms:2-ethoxy-4-nitrobenzaldehyde;1134-43-6;benzaldehyde,2-ethoxy-4-nitro-;SCHEMBL1669597;DTXSID20599688;LMFJUKPFHRKMED-UHFFFAOYSA-N;DB-217313

Suppliers and Price of 2-Ethoxy-4-nitrobenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 2-Ethoxy-4-nitrobenzaldehyde

Chemical Property:

XLogP3:1.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:195.05315777
Heavy Atom Count:14
Complexity:213

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC1=C(C=CC(=C1)[N+](=O)[O-])C=O

Technology Process of 2-Ethoxy-4-nitrobenzaldehyde

There total 4 articles about 2-Ethoxy-4-nitrobenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 10473-47-9
2-Ethoxy-4-nitro-benzylalkohol

: 1134-43-6
2-ethoxy-4-nitro-benzaldehyde

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 4h;

Reference yield:

: 2486-66-0
2-ethoxy-4-nitrobenzoic acid

: 1134-43-6
2-ethoxy-4-nitro-benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: dimethylsulfide borane complex / water; tetrahydrofuran / 5.42 h / 0 - 20 °C / Inert atmosphere

2: manganese(IV) oxide / chloroform / 2.5 h / Reflux; Inert atmosphere

With manganese(IV) oxide; dimethylsulfide borane complex; In tetrahydrofuran; chloroform; water;
DOI:10.1021/jm501532z