cis-1-<2-(2-thienyl)ethyl>-3-methyl-4-piperidine

Base Information

Chemical Name:cis-1-<2-(2-thienyl)ethyl>-3-methyl-4-piperidine
CAS No.:101344-64-3
Molecular Formula:C₂₁H₂₇FN₂O₂S
Molecular Weight:390.522
Hs Code.:

cis-1-<2-(2-thienyl)ethyl>-3-methyl-4-<N-(2-fluorophenyl)-2-methoxyacetamido>piperidine

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis-1-<2-(2-thienyl)ethyl>-3-methyl-4-piperidine

Chemical Property:

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Technology Process of cis-1-<2-(2-thienyl)ethyl>-3-methyl-4-piperidine

There total 12 articles about cis-1-<2-(2-thienyl)ethyl>-3-methyl-4-piperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 348-54-9
2-Fluoroaniline

: 101344-64-3,101344-70-1,101344-72-3,130149-94-9,130149-95-0
trans-1-<2-(2-thienyl)ethyl>-3-methyl-4-piperidine

Guidance literature:: Multi-step reaction with 5 steps

1: p-toluenesulfonic acid / toluene / Heating

2: NaBH₄ / methanol / Ambient temperature

3: 99 percent / tetrahydrofuran / 48 h / Ambient temperature

4: 45 percent / H₂ / 10percent Pd/C / ethanol / 18 h / 2585.7 - 3102.9 Torr

5: Na₂CO₃, NaI / various solvent(s)

With sodium tetrahydroborate; hydrogen; sodium carbonate; toluene-4-sulfonic acid; sodium iodide; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; toluene;
DOI:10.1021/jm00172a032

Reference yield:

: 34737-89-8
1-Benzyl-3-methyl-4-piperidon

: 101344-64-3,101344-70-1,101344-72-3,130149-94-9,130149-95-0
trans-1-<2-(2-thienyl)ethyl>-3-methyl-4-piperidine

Guidance literature:: Multi-step reaction with 5 steps

1: p-toluenesulfonic acid / toluene / Heating

2: NaBH₄ / methanol / Ambient temperature

3: 99 percent / tetrahydrofuran / 48 h / Ambient temperature

4: 45 percent / H₂ / 10percent Pd/C / ethanol / 18 h / 2585.7 - 3102.9 Torr

5: Na₂CO₃, NaI / various solvent(s)

With sodium tetrahydroborate; hydrogen; sodium carbonate; toluene-4-sulfonic acid; sodium iodide; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; toluene;
DOI:10.1021/jm00172a032

Reference yield:

: 348-54-9
2-Fluoroaniline

: 101344-64-3,101344-70-1,101344-72-3,130149-94-9,130149-95-0
cis-1-<2-(2-thienyl)ethyl>-3-methyl-4-piperidine

Guidance literature:: Multi-step reaction with 5 steps

1: p-toluenesulfonic acid / toluene / Heating

2: NaBH₄ / methanol / Ambient temperature

3: 99 percent / tetrahydrofuran / 48 h / Ambient temperature

4: 45 percent / H₂ / 10percent Pd/C / ethanol / 18 h / 2585.7 - 3102.9 Torr

5: Na₂CO₃, NaI / various solvent(s)

With sodium tetrahydroborate; hydrogen; sodium carbonate; toluene-4-sulfonic acid; sodium iodide; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; toluene;
DOI:10.1021/jm00172a032