ClZr(N(2,4,6-trimethylphenyl)PiPr₂)3CoI

Base Information

Chemical Name:ClZr(N(2,4,6-trimethylphenyl)PiPr₂)3CoI
CAS No.:1190919-97-1
Molecular Formula:C₄₅H₇₅ClCoIN₃P₃Zr
Molecular Weight:1063.61
Hs Code.:

ClZr(N(2,4,6-trimethylphenyl)PiPr<sub>2</sub>)3CoI

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ClZr(N(2,4,6-trimethylphenyl)PiPr₂)3CoI

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Technology Process of ClZr(N(2,4,6-trimethylphenyl)PiPr₂)3CoI

There total 8 articles about ClZr(N(2,4,6-trimethylphenyl)PiPr₂)3CoI which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1190919-94-8
ZrCl(N(2,4,6-trimethylphenyl)P(iPr)2)3

: cobalt(II) iodide

: 1190919-97-1
ZrCl(N(2,4,6-trimethylphenyl)P(iPr)2)3CoI

Guidance literature:: In dichloromethane; (inert atm.); stirring mixt. of zirconium compd. and cobalt diiodide in CH2Cl2 at room temp. for 48 h; filtration through celite, evapn., washing with pentane, drying in vac.,elem. anal.;
DOI:10.1021/ic900552b

Reference yield: 67.1%

: 1426099-49-1
ClZr(MesNPiPr₂)₃Co(CO)

: 7553-56-2,12190-71-5,8031-47-8
iodine

: 1190919-97-1
ClZr(MesNPiPr₂)₃CoI

Guidance literature:: In benzene-d6; for 3.75h; UV-irradiation;
DOI:10.1021/ic302473j

Reference yield:

: 1204007-60-2
(THF)Zr(MesNPiPr₂)₃Co

: 1190919-97-1
ClZr(MesNPiPr₂)₃CoI

Guidance literature:: Multi-step reaction with 6 steps

1: tetrahydrofuran / Schlenk technique

2: tetrahydrofuran / 0.25 h / Inert atmosphere; Schlenk technique

3: toluene / 0.17 h / Inert atmosphere; Schlenk technique

4: toluene / Inert atmosphere; Schlenk technique

5: benzene-d6; diethyl ether / Inert atmosphere; Schlenk technique

6: benzene-d6 / 3.75 h / UV-irradiation

In tetrahydrofuran; diethyl ether; benzene-d6; toluene;
DOI:10.1021/ic302473j