ZrCl(N(2,4,6-trimethylphenyl)P(iPr)2)3

Base Information

Chemical Name:ZrCl(N(2,4,6-trimethylphenyl)P(iPr)2)3
CAS No.:1190919-94-8
Molecular Formula:C₄₅H₇₅ClN₃P₃Zr
Molecular Weight:877.709
Hs Code.:

Synonyms:ZrCl(N(2,4,6-trimethylphenyl)P(iPr)2)3

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Chemical Property of ZrCl(N(2,4,6-trimethylphenyl)P(iPr)2)3

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Technology Process of ZrCl(N(2,4,6-trimethylphenyl)P(iPr)2)3

There total 1 articles about ZrCl(N(2,4,6-trimethylphenyl)P(iPr)2)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.4%

: 1168062-59-6
(2,4,6-trimethylphenyl)NHPⁱPr₂

: 10026-11-6
zirconium(IV) chloride

: 1190919-94-8
ZrCl(N(2,4,6-trimethylphenyl)P(iPr)2)3

Guidance literature:: With CH₃CH₂CH₂CH₂Li; In diethyl ether; hexane; byproducts: LiCl; (inert atm.); addn. of hexanes soln. of butyllithium to ethereal soln. of amine deriv. at -78°C over 10 min, warming to room temp., stirring for 2 h, addn. of zirconium compd. at -78°C, stirring for 12 h at room temp.; evapn., extn. (CH2Cl2), filtration through celite, concg., layering withpentane, cooling to -35°C, isolation of crystals, elem. anal.;
DOI:10.1021/ic900552b

Reference yield: 79.0%

: 1190919-94-8
ZrCl(N(2,4,6-trimethylphenyl)P(iPr)2)3

: cobalt(II) iodide

: 1190919-97-1
ZrCl(N(2,4,6-trimethylphenyl)P(iPr)2)3CoI

Guidance literature:: In dichloromethane; (inert atm.); stirring mixt. of zirconium compd. and cobalt diiodide in CH2Cl2 at room temp. for 48 h; filtration through celite, evapn., washing with pentane, drying in vac.,elem. anal.;
DOI:10.1021/ic900552b