C₄₇H₅₄N₂O₁₀

Base Information

Chemical Name:C₄₇H₅₄N₂O₁₀
CAS No.:1330579-34-4
Molecular Formula:C₄₇H₅₄N₂O₁₀
Molecular Weight:806.953
Hs Code.:

C<sub>47</sub>H<sub>54</sub>N<sub>2</sub>O<sub>10</sub>

Synonyms:

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Chemical Property of C₄₇H₅₄N₂O₁₀

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Technology Process of C₄₇H₅₄N₂O₁₀

There total 12 articles about C₄₇H₅₄N₂O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1255790-55-6
(2S,3S,4S,6S)-6-(8-((2R,4R,5S,6R)-5-(benzyloxy)-4-(dimethylamino)-6-methyltetrahydro-2H-pyran-2-yl)-2-((E)-but-2-en-2-yl)-11-hydroxy-7,12-dimethoxy-5-methyl-4-oxo-4H-naphtho[2,3-h]chromen-10-yl)-4-(((benzyloxy)carbonyl)amino)-2,4-dimethyltetrahydro-2H-pyran-3-yl acetate

: 1330579-34-4
C₄₇H₅₄N₂O₁₀

Guidance literature:: With methanol; potassium carbonate; Inert atmosphere;
DOI:10.1016/j.tet.2011.05.117

Reference yield:

: 1255790-48-7
(E)-1''-(5'-((2R,4R,5S,6R)-5-benzyloxy-4-dimethylamino-6-methyltetrahydro-2H-pyran-2-yl)-9',10'-dimethoxy-1'-methoxymethoxy-3'-methyl-8'-(triisopropylsilyloxy)anthracen-2'-yl)-4''-methylhex-4''-en-2''-yn-1''-one

: 1330579-34-4
C₄₇H₅₄N₂O₁₀

Guidance literature:: Multi-step reaction with 4 steps

1: ethanol / 3 h / 20 °C / Inert atmosphere

2: lithium tetrafluoroborate; water / acetonitrile / 0.25 h / 82 °C / Inert atmosphere; Microwave irradiation

3: calcium sulfate; scandium tris(trifluoromethanesulfonate) / 1,2-dichloro-ethane / 67.5 h / -30 - 0 °C / Inert atmosphere

4: methanol; potassium carbonate / Inert atmosphere

With methanol; calcium sulfate; lithium tetrafluoroborate; water; potassium carbonate; scandium tris(trifluoromethanesulfonate); In ethanol; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1016/j.tet.2011.05.117

Reference yield:

: 1273031-50-7
(2R,4R,5S,6R)-5-benzyloxy-2-(6-benzyloxy-5,10-dimethoxy-8-methyl-4-(triisopropylsilyloxy)anthracen-1-yl)-N,N,6-trimethyltetrahydro-2H-pyran-4-amine

: 1330579-34-4
C₄₇H₅₄N₂O₁₀

Guidance literature:: Multi-step reaction with 9 steps

1.1: pyridine; 20% palladium hydroxide on carbon; hydrogen / methanol; ethyl acetate / 2 h

2.1: N-Bromosuccinimide / dichloromethane / 4 h / -78 - 20 °C / Inert atmosphere

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.42 h / 0 - 20 °C / Inert atmosphere

4.1: tert.-butyl lithium / tetrahydrofuran; pentane / 0 h / -78 °C / Inert atmosphere

4.2: -78 - 20 °C / Inert atmosphere

4.3: 20 °C / Inert atmosphere

5.1: barium manganate / benzene / 3.5 h / 20 °C / Inert atmosphere

6.1: ethanol / 3 h / 20 °C / Inert atmosphere

7.1: lithium tetrafluoroborate; water / acetonitrile / 0.25 h / 82 °C / Inert atmosphere; Microwave irradiation

8.1: calcium sulfate; scandium tris(trifluoromethanesulfonate) / 1,2-dichloro-ethane / 67.5 h / -30 - 0 °C / Inert atmosphere

9.1: methanol; potassium carbonate / Inert atmosphere

With pyridine; methanol; calcium sulfate; N-Bromosuccinimide; lithium tetrafluoroborate; barium manganate; 20% palladium hydroxide on carbon; water; hydrogen; tert.-butyl lithium; sodium hydride; potassium carbonate; scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; methanol; ethanol; dichloromethane; ethyl acetate; 1,2-dichloro-ethane; acetonitrile; mineral oil; pentane; benzene;
DOI:10.1016/j.tet.2011.05.117