bis(pentafluorophenyl)(4-nonafluorobiphenyl)boron acetonitrile acetonitrile solvate

Base Information

Chemical Name:bis(pentafluorophenyl)(4-nonafluorobiphenyl)boron acetonitrile acetonitrile solvate
CAS No.:1144521-93-6
Molecular Formula:C₂H₃N*C₂₆H₃BF₁₉N
Molecular Weight:742.15
Hs Code.:

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Chemical Property of bis(pentafluorophenyl)(4-nonafluorobiphenyl)boron acetonitrile acetonitrile solvate

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Technology Process of bis(pentafluorophenyl)(4-nonafluorobiphenyl)boron acetonitrile acetonitrile solvate

There total 2 articles about bis(pentafluorophenyl)(4-nonafluorobiphenyl)boron acetonitrile acetonitrile solvate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1144521-86-7
4-(perfluoro biphenyl) magnesiumbromide

: 344-04-7
bromopentafluorobenzene

: 109-63-7
boron trifluoride diethyl etherate

: 75-05-8,26809-02-9
acetonitrile

: 1144521-93-6
bis(pentafluorophenyl)(4-nonafluorobiphenyl)boron acetonitrile acetonitrile solvate

Guidance literature:: With Mg; In diethyl ether; (N2); addn. of C6F5Br to Mg in ether, stirring for 1 h, soln. filtration, addn. to a soln. of BF3*O(CH2CH3)2 in ether at 0°C, warming to room temp., stirring for 2 h, evapn., addn. of soln. of magnesium compd., stirring overnight at room temp.; evapn. under vacuum, extn. with warm (40°C) light petroleum, solvent distilling off, crystn. from a mixture of acetonitrile and light petroleum at -27°C, elem. anal.;
DOI:10.1039/b817252h

Reference yield:

: 1144521-86-7
4-(perfluoro biphenyl) magnesiumbromide

: 123168-21-8
bis-(pentafluoro phenyl) fluoro borane

: 1144521-93-6
bis(pentafluorophenyl)(4-nonafluorobiphenyl)boron acetonitrile acetonitrile solvate

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether

2: acetonitrile

In diethyl ether; acetonitrile;
DOI:10.1039/b817252h