ethyl(2-carboxymethoxy-5-chlorophenyl)hydroxy acetate

Base Information

Chemical Name:ethyl(2-carboxymethoxy-5-chlorophenyl)hydroxy acetate
CAS No.:76322-34-4
Molecular Formula:C₁₄H₁₇ClO₆
Molecular Weight:316.738
Hs Code.:

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Chemical Property of ethyl(2-carboxymethoxy-5-chlorophenyl)hydroxy acetate

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Technology Process of ethyl(2-carboxymethoxy-5-chlorophenyl)hydroxy acetate

There total 5 articles about ethyl(2-carboxymethoxy-5-chlorophenyl)hydroxy acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 64-17-5
ethanol

: 76322-38-8
(2-carboxymethoxy-5-chlorophenyl)hydroxyacetic acid

: 76322-34-4
ethyl(2-carboxymethoxy-5-chlorophenyl)hydroxy acetate

Guidance literature:: With sulfuric acid; Heating;
DOI:10.1002/bscb.19800890607

Reference yield:

: 17798-46-8
(4-chloro-2-formyl-phenoxy)-acetic acid ethyl ester

: 76322-34-4
ethyl(2-carboxymethoxy-5-chlorophenyl)hydroxy acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / lithium chloride, potassium hydroxide / dioxane; H₂O / 1.) pH=12, 24 h, 5-10 deg C 2.) 24 h, 30-35 deg C

2: 55 percent / sulfuric acid / Heating

With potassium hydroxide; sulfuric acid; lithium chloride; In 1,4-dioxane; water;
DOI:10.1002/bscb.19800890607

Reference yield:

: 90-02-8
salicylaldehyde

: 76322-34-4
ethyl(2-carboxymethoxy-5-chlorophenyl)hydroxy acetate

Guidance literature:: Multi-step reaction with 4 steps

1: 54 percent / chlorine

2: 60 percent / potassium carbonate, potassium iodide / 4 h / Heating

3: 73 percent / lithium chloride, potassium hydroxide / dioxane; H₂O / 1.) pH=12, 24 h, 5-10 deg C 2.) 24 h, 30-35 deg C

4: 55 percent / sulfuric acid / Heating

With potassium hydroxide; sulfuric acid; chlorine; potassium carbonate; potassium iodide; lithium chloride; In 1,4-dioxane; water;
DOI:10.1002/bscb.19800890607