bis(2-diphenylphosphanyl phenyl) ether monosulfide

Base Information

Chemical Name:bis(2-diphenylphosphanyl phenyl) ether monosulfide
CAS No.:1235408-51-1
Molecular Formula:C₃₆H₂₈OP₂S
Molecular Weight:570.631
Hs Code.:

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Chemical Property of bis(2-diphenylphosphanyl phenyl) ether monosulfide

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Technology Process of bis(2-diphenylphosphanyl phenyl) ether monosulfide

There total 1 articles about bis(2-diphenylphosphanyl phenyl) ether monosulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 166330-10-5
bis[2-(diphenylphosphino)phenyl] ether

: C₃₆H₂₈OP₂S₂

: 1235408-51-1
bis(2-diphenylphosphanyl phenyl) ether monosulfide

Guidance literature:: With sulfur; In tetrahydrofuran;
DOI:10.1016/j.jorganchem.2010.10.022

Reference yield: 82.0%

: 16925-25-0
sodium hexafluoroantimonate

: bis(η3-allyl-μ-chloropalladium(II))

: 1235408-51-1
bis(2-diphenylphosphanyl phenyl) ether monosulfide

: [Pd(η3-C3H5)(DPEphos(S))][SbF6]

Guidance literature:: In dichloromethane; N2; stoich. mixt., ligand added to DCM soln. of Pd compd., NaSbF6 added,mixt. stirred for 6 h at room temp.; filtered (Celite), evapd., recrystd. (DCM layered with ether or pentane);
DOI:10.1016/j.jorganchem.2010.10.022

Reference yield: 72.0%

: 16369-40-7
dicarbonyldichlororuthenium(II)

: 1235408-51-1
bis(2-diphenylphosphanyl phenyl) ether monosulfide

: Ru(CO)2Cl₂(bis(2-diphenylphosphanylphenyl)ether monosulfide)

Guidance literature:: In methanol; dichloromethane; under Ar; Ru-compd. dissolved in CH3OH, monosulfide-compd. dissolved in CH2Cl2, solutions mixed together, heated at reflux for 2 h; solv. removed, washed with Et2O, recrystallized from CH2Cl2/Et2O, elem. anal.;
DOI:10.1002/ejic.200901101